GCMS analysis results for sample AD27764, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27764.D Vial: 7 Acq On : 19 Dec 2001 12:38 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 16 1,4-Pentadien-3-ol Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

10.82 0.68 ng/uL 171093 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative. ID MW MolForm CAS# Qual

1 1,4-Pentadien-3-ol 84 C5H80 000922-65-6 33 2 3-Methyl-1-[ (1H)-1, 2,4-triazol-1-yl 153 C7H11N30 064922-02-7 9 3 Hexane, 4-e 1-2,2-dimethyl- 142 C10H22 052896-99-8 9 4 Octane 1 114 C8H18 000111-65-9 9 Abundance Scan 652 (10.818 min): 27764.D (-) m/ 43.10 100.00% 43 83 55 5000-

71 TT 10.40 10.60 10.80 11.00 11.20 . . ........ — • ■ i • I 80 "I" 90 1 ilO 12? 130 140 150 160 m/z 83.05 74.79% m/z~> 20 30 40 50 60 70 Abundance #554: 1,4-Pentadien-3-ol 55 83 A1 1 ' i 5000- 39 27 10.40 10.60 10.80 11.00 11.20 m/ Z 55.10 63.94% 65 | — ' I ' ' ' ' I ' m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10506: 3-Methy!-1-[(1H)-1,2,4-triazol-1-yl]butan-2-one 43 83 TPr 10.40 10.60 10.80 11.00 11.20 5000 71 m/z 41.10 28.12%

55 i 154 ' i ' ■ ■ ■ i' ■ ■ ‘ i' • ■ ' i ■' 1 ■ i' ■ ■ ■ r ■ ■ ■ i' ■ • ' i ' ■ ■ ■ i ■ ■ ■' i ■ ■ ■ ■ i ■ ' ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ' ■ ■ ■ i ■ m/z-> 20 30 40 50__ 60 70 80 90 100 110 120. 130 140 150 160 Abundance #8104: Hexane, 4-ethyl-2,2-dimethyl- W T■ ■ ■ j _ . i 'J 7—.. r~rA _ ।, । . । • । । i TrT 43 57 10.40 10.60 10.80 11.00 11.20 m/ z 58.10 16.53% 5000

27 71 - 1 11 1 ' ..,1.. 85........ 127 AAA m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 10.40 10.60 10.80 11.00 11.20

27764.D NP112701.M Thu Dec 20 11:43:51 2001 Page 16

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