GCMS analysis results for sample AD27639, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\27639.D Vial: 3 Acq On 18 Dec 2001 5:44 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 16 1,4-Pentadien-3-ol Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

10.83 0.62 ng/uL 141345 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Pentadifen-3-ol 84 C5H80 000922-65-6 47 2 3-Methyl-1- [(1H)-1,2,4-triazol-1-yl 153 C7H11N30> 064922-02-7 33 3 Cyclohexane, azido- 125 C6H11N3 019573-22-9 33 4 Cyclohexane, bromo- 162 C6HllBr 000108-85-0 33 Abundance 6 Scan 653 (10.829 min): 27639.D (-) m/z 43.10 100.00% 43 83 55 5000 71 V II 10.40 10.60 10.80 11.00 11.20 — 11 1 1 1 1 1 1 1 T m/z .83.05 74.37% m/z--> 20 30 40 50 60 70 80 90 100 1W 120 130 140 150 160 Abundance #554: 1,4-Pentadien-3-ol 55 83

A - 5000 39 10.40 10.60 10.80 11.00 11.20 27 m/ Z 55.1.0 65.24% 65 ...... —....... — 80 ‘ 90 100 110 120 130 140 150 160 m/z-> 20 30 40 50 60 70 Abundance #10506: 3-Methyl-1-[(1H)-1,2,4-triazol-1-yl]butan-2-one 43 83 Mtr ----- 10.40 10.60 10.80 11.00 11.20 5000- 71 m/ z 41.10 28.77%

55 ■ ।. > ■ ■ । ■ 11 li —........................................ 154 miz—> 20 30 4G 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #4321: Cyclohexane, azido- । r i TTT । i 83 10.40 10.60 10.80 11.00 11.20 55 m/z 71.05 21.91% 41 5000 27 67 96 ' i •' ■ ■ i ■ • ■ ITT , i 11 I1 - 125 i ' ■ ' ' i ' -----AA-AA— m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 10.40 10.60 10.80 11.00 11.20

27639.D NP112701.M Thu Dec 20 11:37:24 2001 Page 16

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