GCMS calibration data, Dec 2001

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Calibration table and response data for GCMS analysis of polycyclic aromatic hydrocarbons dated December 2001.

NYC-WTC_000035350–000035364

Folder label: “GCMS X 11/26/01 A 12/22/01”

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Data File : C:\HPCHEM\1\DATA\DEC210128171.D Vial: 37 Acq On : 22 Dec 2001 1:59 pm Operator: GALOS Sample : gems unknown 11/26 Inst. : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 4 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.23 0.54 ng/uL 142083 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2-methyl-3-propyl- , cis- 100 C6H120 006124-90-9 10 2 1-Butanol, 4- (1-methylethoxy)- 132 C7H16O2 031600-69-8 10 3 CH2=CHCH2C/O)OCH3 100 C5H802 003724-55-8 9 4 Pentanal,/2-methyl- 100 C6H120 000123-15-9 9 Abundance / Scan 587 (10.227 min): 28171.D(-) m/z 43.10 100.00% 43

5000 55 59

39 73 85 9.80 11— r ' 10.00 > — I —A 10.20 10.40 10.60 + — —— - 89 100 . 11।. 111 TTTT 1111111 ■ m/ z 40.86% m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 59.10 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- I 43

57 5000- 71 85 T T* III 9.80 10.00 10.20 10.40 10.60 m/z 39.18% 100 55 ■ 10 j - »■।j • • ■ ■ । ■ ■ ।11 ■' i ■ ■ ■1 i ■ • ■ • । l""l" TT m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #5820: 1-Butanol, 4-(1-methylethoxy)- 43 T A 1.1 4 55 9.80 10.00 10.20 10.40 10.60 73 5000 m/ z 41.10 .3 3.94% I 89 59 ■ i : I Ij . 1 । i I 102 * 11' ‘ ' i ■ ■ ■ ■ i ■ • ■ • i ■ ■ ■ ■ i ■ " ■ i ■ " ■ TTTT ‘I ।' 1111 miz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1448: CH2=CHCH2C(O)OCH3 An- 413 9.80 10.00 10.20 10.40 10.60 m/z 57.1.0 31.18% 5000

39 58 72 100 > I । । > ■ | । । ‘ I । I ! ' i " ’ ■ i " " i ■ " ■ i " " i ■ " ■ i ■1 " i' ■ " i11 " TTTTTT > >!11!!' '('i । TIPIIT 1 -AP— • ■ I ■ ■ miz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 9.80. 10.00 10.20 10.40 10.60

28171.D NP112701.M Fri Dec 28 09:07:41 2001 Page 4

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