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GCMS analysis results for sample AD27679, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27679 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033263–000033284

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27679. D Vial: 6 Acq On : 19 Dec 2001 11:43 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library - : C:\DATABASE\NBS75K.L

Peak Number 11 Hexane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

10.29 5.26 ng/uL 1166070 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane, 2-methyl- 100 C7H16 000591-76-4 35 2 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 25 3 Oxirane, 2-methyl -3-propyl - , cis- 100 C6H120 006124-90-9 23 4 Pentane, 2,3,3 -trimethyl - 114 C8H18 000560-21-4 23 'Abundance ‘ Scan 594 (10.286 min): 27679.D (-) m/ z 43.10 100.00% 43

5000- 57 -............ — — , 85 39 73 10.00 10.20 10.40 10.60

m/z-> 53 —+ HP3—61.-7 100 *——0111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 r m/z 57.10 31.39% Abundance #63434: Hexane, 2-methyl- 43

5000 TIT TPr 10.00 10.20 10.40 10.60 57 85 29 m/z 59.10 28.90% 39 p-mr I - TTTTur 69 100 TTTTTTT ।"1 ■ । TTPTTTTTUTTTT r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #8516: Hexane, 1-propoxy- 43 .............. — '1 11 10.00 10.20 10.40 10,60 5000- m/ z 41.10 28.44% 56 85 39 73 ■ ■ r ■ " i' i r ' " r ' ■' i I' " ' I 1 61 p-m-p-n , 11" ' 111 69 I' " ' I " '' I'''' I'' " I " " I'" ' I r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- ------------------- 48 10.00 10.20 10.40 10.60 m/z 55.10 27.94% 57 5000 71 85

m/z-> - i TTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 rrrf"IrTTT 100 11 ‘1!' I'" TT 11 TIT -4 10.00 10.20 10.40 10.60

27679.D NP112701.M Thu Dec 20 11:42:22 2001 Page 11

NYC-WTC_000033281

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