GCMS analysis results for sample AD27985, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27985.D Vial: 26 Acq On : 21 Dec 2001 6:45 am Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Pentanol, 2,4-dimethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.76 0.41 ng/uL 131634 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 - Pentanol ,/2, 4-dimethyl - 116 C7H160 000600-36-2 33 2 3-Pentano 1, 3-methyl- 102 C6H140 000077-74-7 33 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 4 1-Butanamine, 3-methyl - 87 C5H13N _______ 000107-85-7 9 Abundance Scan 318 (7.759 min): 27985.D (-) m/z 73.05 100.00% 73

5000 43

............ ,1.1 1 55.... .j 87 103 7.40 7.60 7.80 8.00 8.20 ' I 1 * 1 ' I ' ' 1 ' 1 1 1 ' 1 I • 1 ' ' I ' ' ' ' I I ' ' TII +-r TI" . T'T 1'11101'53 , T m/z 43.10. 31.249 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64349: 3-Pentanol, 2,4-dimethyl- 73

5000 55 7.40 7.60 7.80 8.00 8.20 43 27 m/z 45.10 12.65% 15 I r ' ' J ' * ’ ' I ' ' ' ‘ I ‘ ' I ’ • ' ‘ I ' 14.......... i ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । ■

miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #53573; 3-Pertanol, 3-methyl- 73 7.40 7.60 7.80 8.00 8.20 5000 m/z 41.10 9.73% 55 27 45 87

-... A.. 39. | ■ i ■ ■ ■ 1 J T r-r-r j > TT t-j-i , TTTT r n-j-t m/z-> 10 20 ' ' 30 40 50 60 70 80 90 100 110 Abundance #63572:3-Pentanol, 3-methyl- 73 7.40 7.60 7.80 8.00 8.20 m/z 71.05 7.26% 5000 55 45

miz-> .......... 271..... , 1..... ------- 1 10 TT - > TIT r i 1n/dB.T TI—T 20 30 40 50 60 70 80 87

90 100 110 , , . .... . A—... 7.40 7.60 7.80 8.00__ 8.20

27985.D NP112701.M Fri Dec 28 09:31:02 2001 Page 5

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