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GCMS analysis results for sample AD28046, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD28046 conducted on January 2, 2002, noting unknown compounds and surrogate recovery.

NYC-WTC_000034484–000034494

Folder label: “GCMS X 11/21/01 A 12/21/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28046.D Vial: 30 Acq On : 21 Dec 2001 9:33 pm Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.71 0.51 ng/uL 170049 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-1methyl - 102 C6H140 000077-74-7 28 2 3-Pentanol, -methyl- 102 C6H140 000077-74-7 25 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane, B-methoxy- 102 C6H140 036839-67-5 9 Abundance ' ” ' Scan 313 (7.712 min): 28046.D (-) m/ z 73.05 100.00% 7(3

5000 43 ........ —......... 1........ 87..........103 7.40 7.60 7.80 8.00 —................... 14 r। . 55 . , . । 1 m/z 43.10 32.32% miz-2 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 ------ 55 7.40 7.60 7.80 8.00 45 87 m/z 40.00 28.28% 27 | I -i-r-j-r-r T-TYT-rTA-jA-rT-r-j-r-rH-r-j-r-r I ' ' ' ' I ' । ' 1 । ' 1TT । । । । । । । । । । । । mz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573; 3-Pentanol. 3-methyl- 73 ........A— 7.40 7.60 7.80 ■ l 1 8.00 ■ I

5000 m/z 44.10 18.94% 55 45 87 27 39. ■I ' ' ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- 73 7.40 -A ..... A— 7.60 7.80 8.00 m/ z 45.10 12.86% 5000

45 TII—B—15 31 m——nm—IPT , .1 55 ..........88..................... miz-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

28046.D NP112701.M Thu Dec 27 08:38:40 2001 Page 1

NYC-WTC_000034492

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