GCMS analysis results for sample AD27622, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27622.D Vial: 22 Acq On : 20 Dec 2001 5:04 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 5 3-Pentanol, 3-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.76 0.95 ng/uL 272059 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Te tive ID MW MolForm CAS# Qual

1 3-Pentanol3-methyl- 102 C6H140 000077-74-7 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 Silane ./ tetramethyl - 88 C4H12Si 000075-76-3 9 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 Abundance Scan 319 (7.765 min): 27622.D (-) m/ z 73.05 100. 00% i 73

5000- 43

miz-> 10 20 30 +40 —TTrmTT 50 55 60 . 1 |...........87............... 1Q3 , 70 80 90 100 110 7.40 m/z 7.60 43.10 7.80 8.00 31.06% 8.20

Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 55 7.40 7.60 7.80 8.00 8.20 45 87 m/z 45.10 12.23%

m/z->10 20 7—... -. .30 40 50 60 I ' I ' 70 I " I ' . I 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73 — 7.40 7.60 7.80 8.00 8.20 5000- m/z 41.05 10.16%

45 15 I 53 I 59 88 -IITTImmmT • ' 1 1 1 । • ■ ■ ■ । ■ • ■ ■ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 'Abundance #845: Silane, tetramethyl- R1—ffT 73 7.40 7.60 7.80 00 3.20 m/z 71.05 7.15% 5000 -

15 31 —————————————— 1 1 I _ 45 55 I.......... 88........................ _ __ LA m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00 8.20

27622.D NP112701.M Fri Dec 21 09:16:53 2001 Page 5

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