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← Document results/DEP Box 22/GCMS X 11/23/01 A 12/21/01
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GCMS analysis results for sample AD28167, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD28167 conducted on January 2, 2002.

NYC-WTC_000034596–000034614

Folder label: “GCMS X 11/23/01 A 12/21/01”

←Page 10 of 19→
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28168.D Vial: 18 Acq On : 22 Dec 2001 10:19 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Hexanone Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

6.40 0.53 ng/uL 138999 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 rentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3 -Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H120 000589-38-8 91 4 3 -Hexanone 100 C6H120 000589-38-8 78 Abundance Scan 169 (6.395 min): 28168.D (-) m/z 43.10 100.00% 43 57

5000

m/z-> M1 |" " r " ■ i 39 +pm8R— 71

•■l ■■ ■ ■l ■ ■■ ■ I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100

। ■ ■ ■■ । A 6.00 m/z 6.20 57.10 A 6.40 6.60 6.80 85.68% Abundance #1528: 3-Hexanone

AW_ 43 57

29 71 5000 -IA4 TT-ODB/IIEIIITTT 6.00 6.20 6.40 6.60 6.80 100 m/z 71.05 53.93% , 85 | ■■r"■r TTTTTTTT ............. I' Wm..... '"I......... . l~" 'I....... " ..........."I miz- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #83357: 3-Hexanone 43 57 —.......... — 29 ITIurrrr 6.00 6.20 6.40 6.60 6.80 5000 71 m/z 100.05 29.31%

1‘........... ‘1‘1‘1T"‘11 j............ ‘3T n-rrphi........... 1............ \............. ‘1111‘E0II—OITOVTTIO"SEII"I"EIEI .. ।.... । ..85 100 ........................ ।.... ।. ri 111111 1111111111 fl m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105_ Abundance #63358: 3-Hexanone ........ / 1 43 6.00 6.20 6.40 6.60 6.80 57 m/z 41.10 27.09% 5000 71

100

I s ■ -r. "T. ■ < ,..|.... | II II. f ,11111111n 11 11111111 , 85 ! 11111 11 IT) III11111 > 111111111 —IAALWNNWA m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

28168.D NP112701.M Fri Dec 28 09:58:57 2001 Page 2

NYC-WTC_000034605

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NYC-WTC_000034605Source: NYC Law Department, mirrored locally

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