GCMS analysis result with unknowns, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26335.D Vial: 17 Acq On : 1 Dec 2001 2:45 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Aziridine, 2,2-dimethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.17 0.63 ng/uL 283242 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Az iridine, 2,2- dimethyl - 71 C4H9N 002658-24-4 25 2 1-HexaAoi 102 C6H140 000111-27-3 9 3 1-Hexanol 102 C6H14O 000111-27-3 9 4 l-Hexanol 102 C6H140 000111-27-3 9

W Abundance 7 Scan 36 (5.170 min): 26335.D (-) m/z 41.05 100.00% 41 59 56

5000 71

m/z—> 5 ..... M.—l 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 i ■ • • < i1 * • ‘! 84 5.00 5.20 ' 5.40 5.60 m/z 59.10 83.17% Abundance #248: Aziridine, 2,2-dimethyl- 35 56 3942 T I I I I I I I I T $ [d I I f I’l 5000 27 71 5.00 5.20 5.40 5.60 15 m/z56.10 74.76%

WA TT I’ Tpp IBtS46111141 miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63562:1-Hexanol 43 55 TIAMM 5.00 5.20 5.40 5.60

A 5000 27 31 m/z 42.05 49.81% 69 15 _ 73 ।84 TTPITI .. .. ।. . . . | . M |I I ,J, I TIT THTP 111»*»• l. mfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #1782:1-Hexanol A AY 56 5.00 5.20 5.40 5.60 43 m/z71.05 34.78%

A 27 31 5000 69 84 73 "1' I “ " i1 ■' ■ i" ■ ■ r 1’1 Hp TTTTp ’ 5.60 m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 5.00 5.20 5.40

26335.D NP112701.M Tue Dec 04 15:07:21 2001 Page 1

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