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GC/MS analysis results for sample AD22549, September 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087022–000087043

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087036
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPC' JM\l\DATA\SEP2601\22549 .D Vial: 3 Acq On : 26 Sep .001 12:17 pm Operator: GALOS Sample : GC/MS ucnown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Pa; ms: LSCINT.P

Quant Method : C:\IIPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L *******************■!:************•*****************•*■*■*■****■*•*■***********

Peak Number 7 Hex;■ e, 2,3,4-trimethyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 30.89 0.49 ng/uL 37615 Chrysene-dl2 33.30

Hit# of 5 Tent; ive ID MW MolForm CAS# Qual

1 Hexahe, 2,3,4 -1 r i:: le t hy 1 - 128 C9H20 000921-47-1 9 2 Heptane 2,3-dim .'thyl- 128 C9H20 003074-71-3 9 3 Hexane, ,3,4-trimethyl- 128 C9H20 000921-47-1 9 4 Azetidine\ 1-methyl- 71 C4H9N 004923-79-9 5 Abundance S • 0841 (30.889 min): 22549.D (-) m/z 57710 100.00% 43 71 5000 85

T 30.60 30.80 31.00 31.20 50^ ■’ 70 80 90 100 110 120 130 m/z 43710 80.39% nfe-> 20 30 40 Abundance # ; i 23: Hexane, 2,3,4-trimethyl- 4)3 ■

5000 57 71 30.60 30.80 31.00 31.20 85 27 m/z 71705 65.16% > I ■ '' 11 11 I 11 I ,,, li ' I I'I I ' I' ' ................................. 128 n/z-> 20 30 40 50 70 80 90 100 110 120 130 Abundance i 33: Heptane, 2,3-dimethyl- 43 ___ l,i........ 30.60 30.80 31.00 31.20 5000 m/z 85.05 43.03% 84 27 71 128 tVz-> 20 30 40 50 50 70 80 90 100 110 120 130 Abundance 47: Hexane. 2,3.4-trimethyl- 43 30.60 30.80 31.00 31.20 m/z 41.10 35.08%

5000 57 71 85

27 L, , , , , I, , , , , , . , 11 , , . , I, I • ( ' ' I . I I ............................... 128 nfe-> 20 30 40 50 e'j 70 80 90 100 110 120 130 30.60 30.80 31.00 31.20

22549.D NP072501.M Mon Oct 01 14:40:30 2001 Page 7

NYC-WTC_000087036

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NYC-WTC_000087036Source: NYC Law Department, mirrored locally

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