GC/MS analysis results for sample AD22549, September 2001

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Library Search Compound Report

Data File : C:\HPCnEM\l\DATA\SEP2601\22549.D Vial: 3 Acq On : 26 Sep 2001 12:17 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Paraias: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 ;S25/TCLP calibration table 7/25/01 Cl IS 5 Library : C: V.-ATABASE\NBS75K.L ********************,>r ************************************************

Peak Number 8 Cyclohexane, (1,1-dimethylethy Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T, 31.82 0.48 ng/uL 36642 Chrysene-dl2 33.30 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 CycDs^exane, (1,1- imethylethyl)- 140 C10H20 003178-22-1 25 2 Piperisdin-4-carbo::- 'lie acid 129 C6H11NO2; 000498-94-2 9 3 .alpha\D-Galactc /ranoside, methyl 176 C7H12O5 005540-31-8 9 4 1-Hexene\ 2,5-dime i. hy1- 112 C8H16 006975-92-4 9 Abundance \ Scan '.043 (31.824 min): 22549.D (-) m/z 56.10 100.00% 5|S

43 5000 73 129 31.40 31.60 31.80 32.00 32.20 I ,11 -b-TT-rp • I “mTz sYTTy; 52.43% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #760 • yclohexane, (1,1-dimethyIethyl)-

5000 41 ' ' I ' 31.40 31.60 31.80 32.00 32.20 67 82 ■m/z 43.10 50.65% 27 I Jill j| . . . 125 . 140 T)/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #5228: Piperidin-4-carboxylic acid 5|5

31.40 31.60 31.80 32.00 32.20 5000 “m/z 41.10 41.6^ 30 84 42 129 .... I 73 100 ' I '' ' ' I ‘ ' I ' ' ' 'I ' ... Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #16579: .alpha.-P-Galactopyranoside, methyl 3,6-anhydro- ■p-TT-r-T-p—r 57 73 ai4g_jr6o_3ijo_3zoo_322g_ 8000 “m/z 55.10. 33.84%

6000 85 102 4000 33

nZz-> 20 30 40 50 s' 470 80 90 100 110 120 130 140 -p-r-r-r-p-r I ' ' ' ' I ' ' 31.40 31.60 31.80 32.00 32.20

22549.D NP072501.M Mon Oct 01 14:40:31 2001 Page 8

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