GC/MS calibration data for sample 28323, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Pentane, 2,2,3,4-tetramethyl- Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

12.51 0.80 ug/1 >03445 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pentane, 2,2,3,4-tetramethyl- 128 C9H20 001186-53-4 59 2 Decane, 2,6,6-trimethyl- 184 C13H28 062108-24-1 50 3 Azetidine, 1-methyl- 71 C4H9N 004923-79-9 47 4 Hexane,2,2,5-trimethyl- 128 C9H20 003522-94-9 45 Abundance / Scan 813 (12.511 min): 28323.D(-) m/z 57.00 100.00%

A S 57

5000 43 71 TTi । | । rr , i । , 88 113 12.20 12.40 12.60 12.80

m/z-> +50, ...................38 1 , 111 1 1 1 1 1 1 1 ■ ‘ 1 ‘I1 20 30 40 50 4 60 70 65,111,77/...... P.11170011111127,.1 80 90__ 100 110 120 130 m/z 43.05 46.77%

AMN Abundance #5164: Pentane, 2,2,3,4-tetramethyl- 57 43 5000 12.20 12.40 12.60 12.80 ‘ 27 71 m/z 56.00 40.24%

N 85 —1 --------- m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance '*19023. Devane, 2,6,6-trimethy 57 rl ‘ • 1 • I ‘ ‘ ‘ ‘ I 4 ’ 1 ‘ ) 12.20 12.40 12.60 12.80 5000 43 m/z 71.00 31.13%

A./UN 71 85 99 127 I ... m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance . #246: Azetidine, 1-methyl- 33 42 12.20 12.40 12.60 12.80 m/z 41.05 30.11%

ANWN 5000 56 71

m/z-> * i' • 20 Hl 30 ■ ■ i 1 40 TT-p-r 50 60 70 80 90 100 110 120 130 12.20 12.40 12.60 12.80 ’ ’1

. 28323.D GCMS1126.M Wed Feb 06 13:01:32 2002 Page 3

NYC-WTC_000018527