NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39
Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T.
36.71 0.87 ug/1 150889 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 43
2 Si] namine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 27
3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25
4 -(3-Hydroxyphenyl)-3-hydroxypropio 398 C18H34O4Si3 000000-00-0 25
Abundance Scan 3450 (36.714 mln): 30985.D (-) m/z 73.00 1 00.00%
73
147
5000
221
281 355 36.40 36.60 36.80 37.00 1
45
TMIr 103 . j 193 253, .327, 1 401 429 .............
I "I । ■ | >1 T । | > । |"1 1 I 1 ( 1 1 T 1 | l I 1 I | I I I T-J-TT m/z 147.00 54.47%
miz->
Abundance
50 100 150 200 250 300 350 400
#74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
450 500 550
73
147
5000
J _
1744 P 1 11 TTnATvf
36.40 36.60 36.80 37.00
281
45 369 m/z 221.0,5 35.16%
— 117 , i 207 249
'T* ‘ * • i
mz—> 50 100 150 ‘ 200 250 300 350 400 450 500 550
Abundance
73
#39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oyj
209
281 A.
36.40 36.60 36.80 37.00
m/z 281.00
1/
19.46%
5000
45 251
120 147 179....
■ • i ‘ ■ i ■ ■ ‘ ‘ i • ■ 1 ■ । ■1 ■ । • ■ • ■) ■ • ■ ■ । ‘ । • i1 ■
m/z-> 50 100 150 200 250 300 350 400 450 500
#60503:3-lsopropoxy-1,1,117,7.7-hexamethyl-3,5,5-tris(trim
550
Abundance ■ ■ ' I ‘ ‘ 1 1 ‘ ‘ 1 1 ‘ ‘ ‘ I ' ‘ ‘ ■ I
73 36.40 36.60 36.80 37.00
m/z 207.01) 15.56%
5000
147 aod Anaw/
221 281
■ ■ । ■ ■ ■ • । • ■ ■ ■ । ■1111 •f । f' । ■ 327... 415. ..5561
350 ' 400 ' ‘ 450 500 550 ‘ 1 ■ i 1 1 ■ ■ I • ■ • 1 133 । । । । > । i f
m/z-> 50 100 150 200 250 300 36.40 36.60 36.80 37.00
30985.D GCMS1126.M Wed Jan 23 08:58:11 2002 Page 15
NYC-WTC_000018283
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