GCMS calibration table for TCLP analysis, February 2002

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Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.

NYC-WTC_000052600–000052606

Folder label: “GCMS X 1/15/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1402\1004.D Vial: 10 Acq On : 14 Feb 2002 6:47 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Decene, 2,4-dimethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.30 1.29 ug/1 90735 Perylene-dl2 38.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Decene, 2,4-dimethyl- 168 C12H24 055170-80-4 25 2 Propanedioig acid, hexyl-, diethyl 244 C13H2404 005398-10-7 12 3 Naphthalene', l-isothiocyanate- 185 C11H7NS 000551-06-4 10 4 Heptadecane, 7-methyl- 254 C18H38 020959-33-5 10 Abundance 7 Scan 3404 (36.297 min): 1004.D(-)................................. |... m/z 185.io 100.00% 155

57 5000 43 70 112 83 98 36.00 36.20 36.40 36.60 125 183 157166 I 207 I"1 ''I " I'' । I rr ........ ..... 'l . " I" " I'" 'I ′′ II ll "'ll" I'..... rI -mmpp m/ Z 57.00 53.08% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 Abundance #14795: 1-Decene, 2,4-dimethyl- 43 57

83 5000 • ■ i ■ 70 36.00 36.20 36.40 36.60 112 m/ z 70. 43.03% 97 168 I i" " I r "' i" " i" " I" " r ■ ■ ■ r'" i' ‘" r'" r ’" I" •' i miz- 30 40 50 60 79 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 Abundance ■ .* 57 70 36.00 36.20 36.40 36.60 5000 112 m/z 55.00 41.88% 83 42 98 199 217 b"dssuoooootoovprosshsoooovooc/*okl6*o*AA**SAVASASA****G****4***A*/S/ " r ■" r "11 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140150 160 170 180 190 200 210 220 Abundance #19180: Naphthalene, 1-isothiocyanato- ‘ I’’ 185 ___ 36.00 36.20 36.40 36.60 _ 153 m/z 71.10 38.12% 5000 127 93 141 ______ ____ I ___ PT + miz-? r." i'" ' r " ' i''' • i" " r "' i"1 ‘ r " ■ i 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 I" " I 4 p-rrrp-rrrj- Tini 36.00 36.20 36.40 36.60

1004.D GCMS0308.M Thu Mar 14 15:28:22 2002 Page 1

NYC-WTC_000052605

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GCMS calibration table for TCLP analysis, February 2002 · Box DEP Box 28

NYC-WTC_000052630

Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.

Same agency, volume and box · similarity 0.995