GCMS analysis report for sample AE01225, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\ 1\DATA\FEB1502\1225.D Vial: 27 Acq On : 16 Feb 2002 6:36 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Pentane, 3-methoxy- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.28 ug/1 23647 1,4-Dichlorobenzene-d4 12.33

Hit# of Tentative ID 5 MW MolForm CAS# Qual |----------------------- 1 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 5 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 4 4 1,4-Butanediamine 88 C4H12N2 000110-60-1 4 Abundance / Scan 345 (8.208 min): 1225.D (-) m/ z.... 73.00 100.00 % ( 3

5000 43

391 । 51 55 59 69, 7.80 8.00 8.20 8.40 8.60 , 86 > । ■ I ■11111■|....,I...|.1. 11. <।। ' 111 > 11 ■ " ' i " " i'''' r ■ " i " m/z 43.05 39.26% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1793: Pentane, 3-methoxy- 73

5000 — I ' 1 ' 1 I ' ' ' — 41 45 7.80 8.00 8.20 8.40 8.60 m/ z 41.0 14.22% 271 . 33 55 59 70 m/Z-> . 5 l""l""i i ■ " • i11 Tsel 111111 < । TTT ++ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance -Ethyltrmam 30 73 ............... .................. 7.80 8.00 8.20 8.40 8.60 5000 m/ z 45.0.5 12.85% 44 58 27 15 41 TIIVPIT 'I""I I'''' I' " ' I " '11" '' I 111''11'1 ’ * I'1' ■ I ‘' I' m/z—> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #62932: Silane, tetramethyl- 73 7.80 8.00 —4 8.20 8.40 8.60 m/ z 71.10 9.37% 5000

45 15 42 i 53 59 88 m/z-> 5 " '11 ■ 10 i ” ’ ■ i ■''' i " ■ ■ i P l ■ ■ i ■ | ■ ■ 111 TITT "1.... 11 'I 1 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1225.D GCMS0208.M Wed Feb 20 14:30:51 2002 Page 1

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