GCMS analysis results for sample AE01043, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1502\1043.D Vial: 29 Acq On : 16 Feb 2002 8:32 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Pentanol, 3-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.35 ug/1 28111 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual ----------- - ------------------ 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 2 Pentane,/3-methoxy- 102 C6H140 036839-67-5 9 3 Butane,/2-methoxy-2-methyl- 102 C6H14O 000994-05-8 9 4 Formamide 7 , N,N-dimethyl- 73 C3H7NO 000068-12-2 5 Abundance c Scan 346 (8.217 min): 1043.D(-) m/ z 73.00100.00% 73

5000 43

7.80 8.00 _ 8.20 . 8.40 8.60

m/z-> ■ r ' ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i' 20 25 30 35 444447+7 mmp .......... . 40 45 50 55 55 60 65 69. 70 75 80 85 .......... 90 95 m/ z 43.05 33.64% Abundance #63573: 3-Pentanol, 3-methvi- 73

5000 55 .A AA4W 7.80 8.00__8.20 8.40 +4r — 8.60 45 87 m/ Z 45.05 12.53% 27 69 •11' ■ ’ ■ । ■ 31 i । h i i । i i .Tti 41 i i |; i i i i । i ' I' " 11 " " I " " I' 84 i ' i ■ ■'' i''' ■ i ■ ■ ■ ■ i ■' ■ ■ i ■

m/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 73

7.80 A 8.00__ 8.20__ 8,40 8.60__ 5000 m/z 41.05 12.25% 41 45

m/z-> Abundance 27 33 55 59 70 1avyssswguutttvssuvsruytovvgvvooi*avogww*II***S**SSAS*I*I*S***I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #63526: Butane, 2-methoxy-2-methyl- 73 ALA 7.80 m/ Z 8.00 8.20 7 0.90 8.40 _8.60 _ 7.62% 5000 55 87

------- 27 31 42 45 no • 70i I T1**1PITTT > i ■ ■ • ■ i ■ ■ ■ ■ i ■ ■ i ■'111 ■ ' ■ i 1 ■ ' ' i ■ ■

miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1043.D GCMS0208.M Wed Feb 20 14:29:24 2002 Page 5

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