GCMS analysis results for sample AE01043, Feb 2002

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GC/MS analysis report for sample AE01043 showing surrogate recovery data generated on February 25, 2002.

NYC-WTC_000052832–000052847

Folder label: “GCMS X 1/17/02 A 2/16/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1502\1043.D Vial: 29 Acq On : 16 Feb 2002 8:32 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

7.23 0.50 ug/1 39664 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Hexanol, (S)- 102 C6H140 052019-78-0 64 4 2-Hexanol, (R) - 102 C6H140 026549-24-6 64 Abundance Scan 238 (7.225 min): 1043.D (-) m/z45.05100.00% 45

5000 —

m/z-> 10 r ■ ■' i'''1 r ■' ■ i ■ ■' ■ i ■ 15 20 25 30 4 51 57 69 I ........ ITTI......... > 1111111 >'111'''11... 11.1.. ।.... ।' 35 40 45 50 55 60 65 70 75 80 85 90 95 84 87 6.80 7.00_ 7.20 m/ z 69.10 7.40 _7.60 13.76% Abundance #83547: 2-Pentanol, 4-methyl- 46

5000 > I ■ 1 ■ ' । > 1 1 > । > 6.80 7.00 7.20 7.40 7.60 27 69 m/ Z 41.05 13.56% 1 38 42, 57 । 84 87 • l ■ ■ • ■ l • •• ■ l • " 11'' " I • " ’ I • ■ ’ ■ I'" 111 • । • • • • 11। ■ ■ • • । ■ ■ ■; ।। ■ ■ ■ • । > ■ • > । ■ i" ■ ’ i • m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 45 - । . r ■ ■ । .. . .A, A, - 6.80 7.00 7.20 7.40 7.60 _ 5000 m/z 43.05 10.26% 69 27 31 39 42 55 58 84 87 m/z-> Abundance 10 ‘I‘*"‘I‘S‘SI‘‘‘IVSLVUV*S*SD‘ 15 20 25 ‘/SC*Tt"B‘‘‘*T" 30 35 40 45 50 55 60 65 #1769: 2-Hexanol, (S)- 45 TWWWWIIWWTPUILUITTTT 70 75 80 85 90 95 6.80 N 7.00 7.20 Trram ‘117* 7.40__ 7.60 m/z 44.00 7.34% 5000

69 84 87 m/z-> .. 18.. ”.. c 55 ■ ■ i ■ ■111' " ' i'''' i'' 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.80 7.00 7.20 7.40 7.60 11" ।■ ' i ■ ■' ■ i ■ " ■ i ■' ■ ■ i ■

1043.D GCMS0208.M Wed Feb 20 14:29:19 2002 Page 4

NYC-WTC_000052842

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NYC-WTC_000052842Source: NYC Law Department, mirrored locally

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