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GCMS analysis results, sample AD25603, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25603 conducted on November 28, 2001, noting unknown compounds.

NYC-WTC_000069790–000069802

Folder label: “GCMS Scan X 10/27/01 An 11/17/01

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Scanned page image, NYC-WTC_000069800
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NYC 9/11 Public Portal Document

Library Search Confound Report Data Pile : C:\HPCHEM\1\DATA\NOV1601\25603.D Vial: 2 Acq On : 16 Nov 2001 4:00 pm Operator: 209 GALOS San^ile : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 2-Pentanol, 4-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.46 ug/1 84468 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanolz^-methyl- 102 C6H14O 000108-11-2 83 2 2-HexanQlr 102 C6H140 000626-93-7 83 3 Hexane< 1-methoxy- 116 C7H16O 004747-07-3 38 4 (R) - -2-Pentanol 88 C5H12O 031087-44-2 36 Abundance Scan 177 (6.666 min): 25603.D (-) m/z 44.95 100.00% 46

5000

41 69 6.^I , 51 5658 I 8487 6.60 6.80 7.00

nfe-> AWi I'' " 1'''' I'' " I''' ’ I ++TTTTT+4+rtrpTTTTTt4|TT^^ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z 69.05 16.98% Abundance #63546:2-Pentanol. 4-methyl- 4"

5000 6.40I 6.60 6.80 7.00 27 m/z :41.05 11.99% 69 42 ... I'''' 111" I'''' I ‘H‘' I''" I'" h'' ‘' I'''' I' TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol 4|5

6.40I 6.60 6.80 7.00 500) m/z 43.05 10.65%

TiZz-> ^bundanc8 10 19..... .................. ,^i ’ ‘ 1 *''' I' ’ ‘ ‘ I''' ‘ I' ‘' I'''' 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #64352: Hexane. 1-methoxy- 4)5 63

.. I................. Ji L 6.^ " 6,^ " eio " 7.00 " ' "inTz 44700 8780% 5000 56

41 69 84 33 ' ‘" I I" I" " I" ‘ h " “ I" " I'" 11" " I ‘' I' I''" I ‘‘' I' ‘ ‘' I ‘' I' ‘ I' I -l-rrrr Tife-> 10 15 20 25 30 35 40 45 50 55 60 70 75 80 85 90 95 6.40 6.60 6.80 7.00

25603.D NP103001.M Tue Nov 27 09:42:45 2001 Page 3

NYC-WTC_000069800

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NYC-WTC_000069800Source: NYC Law Department, mirrored locally

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