GCMS analysis results for sample AE01403, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1902\1403.D Vial: 12 Acq On : 19 Feb 2002 9:05 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.33 ug/1 23083 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 / Tentative ID MW MolForm CAS# Qual _/___________________ 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 2 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 3 1,3-pioxolane 74 C3H602 000646-06-0 4 4 Formamide, N,N-dimethy1- 73 C3H7NO 000068-12-2 4 Abundance Scan 344 (8.204 min): 1403.D (-) m/ z 73.00100.00% 73

5000 43 40

miz-> 20 25 30 35 4 40 45 50 55 69, —pH— 111IIPTTI 87

55 60 65 70 75 80 85 90 95 7.80 m/z 8.00__ 8.20 43.05 8.40 8.60 _ 31.67% Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 55 7.80__ 8.00 8.20__ 8.40 8.60

27 31 42 45 69 87 m/z 39.95 23.855 59 84 | ■ ■ i ■ ' i' ' ■ ■ i' ■'' i' ■ ■' i'''' i ■ ■' ■ i' 11WWPPPmu]m T/Z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 73

55 7.80 8.00 8.20 8.40 8.60 43 5000 m/ z 41.0.5 13.61% 27 31 70 81 ' ■ i ■' ' ■ i1 ' ■ • r ■'' i ■ ■' ■ i ■' ■' i ■' ■ ■ r ■ ■' i ■ ■ ■' i' ■ ■' i' ■ ■' i ■ ■ ■ ■ i' ■ i'1' ■ i ■1 ■11 ■' ■ • i • m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #320: 1,3-Dioxolane 73 7.80 8.00 8.20 8.40 _8.60 _ m/z 45.05 13.61% 29 44 5000

-1 ■i■1'■I'’11 ■ • ■ i ■' ■ ■ i ■ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1403.D GCMS0208.M Thu Feb 21 15:29:35 2002 Page 1

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