GCMS analysis results for sample AD31407, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report > Data File : C:\HPCHEM\1\DATA\JANI602\31407.D Vial: 7 Acq On : 16 Jan 2002 5:30 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.44 3.38 ug/1 825727 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 102 C6H140 000994-05-8 9 3 Butane,/2 -methoxy-2 -methyl - 4 Penta: , 3-methoxy­ Abundance Scan 261 (7.445 min): 31407.D (-) 73 102 C6H140 m/z T 036839-67-5 9

5000 43 > i • • • > j > < • < । • 7.20 7.40 7.60 7.80 0- • ■ । ‘ ‘ । 1 । ■ ,38,11,1, ,50,-5590, 67+, l > ■ । ■ ‘ “'i 1*I**I4 , 87 103 m/z 43.00 34.92% miz-> 10 20 30 40 ' 50 60 __ 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 • • • • | 4 ■ • • 1 • • • . | | ' ‘ ‘ 55 7.20 7.40 7.60 7.80 45 87 m/z 45.05 12.22% ■ 27 • • । • • » > । • i' • • ■ ' l 1 r -Pr 1 1 1 i 1 1 ' 11 1 1 ' ' i ■ 1 • ' i ■ ■ ■ ■ i ■ ■ ' 1 i ' miz-> 10 20 30 40 50 60 70 80 90 100 110 [Abundance #62932: Silane textramethvl- 73 , r / — 1 । ■ TPt IT 7.20 7.40 7.60 7.80 5000 m/z 41.00 12.11% 45 15 | 53 59 .....88.... ■ ■ i ■ ' 1 ■ i ■ ■ ■ ■ i ■ ■ • ■ i • ■ ■ • i ■ ■ ■ ‘ i ■ 1 ■ ■ i • ■

m!z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- Kummmmmoffror 73 7.20 7.40 7.60 7.80 m/z 71.00 6.99% 5000 55 87 45 27 33 ■ i ■ ' TIIBmmT *1121114**18***** 1 • ■ i ■ • ‘ 1 i ■ ' ■ • i ■ ■ ■ ■ i • ■ ' i ■ ‘ ■ i • ■ ■ ■ i • ‘ miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31407.D GCMS0103.M Thu Feb 07 09:16:42 2002 Page 1

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