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GCMS analysis results for sample AD31407, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31407 conducted on February 13, 2002.

NYC-WTC_000018048–000018057

Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01

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Scanned page image, NYC-WTC_000018056
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NYC 9/11 Public Portal Document

Library Search Compound Report 8 Data File : C:\HPCHEM\1\DATA\JAN1602\31407.D Vial: 7 Acq On : 16 Jan 2002 5:30 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.58 0.64 ug/1 156674 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 33 2 1-Octadecanol 270 C18H380 000112-92-5 9 3 2-Acetylthiazole 127 C5H5NOS 024295-03-2 5 4 N-A tylpyrrolidone 127 C6H9NO2 000932-17-2 4 Abundance Scan 276 (7.582 min): 31407.D (-) m/z 4 .05 100.00% 43

5000 ............. . ................................. , 63 82 97 127 7.20 7.40 7.60 7.80 8.00 | m/z~> 44’14 20 ushomposisshpur 11aa*,a***)***22**** 40 60 80 100 120 140 160 180 200 220 240 260 m/z 126.90 7.97% Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 7.20 7.40 7.60 7.80 8.00 15 m/z 46.95 6.90% 85 97 125 । । < । • r। > j • miz->_ _ 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance 43 #72027 1g0lspand! wwrMw Wwww 7.20 7.40 7.60 7.80 * 8.00 5000 82 m/z 124.8 6.52% 56 68 97 j i | 111 125 224 270 I I | > 1 I I| > TI i l rih I I I I I I I i I I I I ■ . > . | > ■ ■ • | > ■ . > |I . > . | I ■ . . | I > ■ ■ | ■ > ■ > | i i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 .... n... Abundance #4717: 2-Acetylthiazole 43 7.20 7.40 7.60 7.80 8.00 m/z 96.90 6.18% L 5000 58 99 127 112 85 I I • •!••••]•>• • । • ■ ■ • । r * ' • p +I*‘‘I‘I**‘I****I* miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 720 7.40 7.60 7.80 8.00

31407.D GCMS0103.M Thu Feb 07 09:16:46 2002 Page 2

NYC-WTC_000018056

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NYC-WTC_000018056Source: NYC Law Department, mirrored locally

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