GCMS analysis results for sample AE01043, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1502\1043.D Vial: 29 Acq On : 16 Feb 2002 8:32 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.12 0.57 ug/1 45559 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 l-Hepteh-4-ol 114 C7H140 003521-91-3 10 3 1-Propanamine, 2-methyl- 73 C4H11N 000078-81-9 9 4 Propane, 2-ethoxy-2-methyl- 102 C6H140 000637-92-3 9 Abundance Scan 226 (7.115 min): 1043.D(-) m/z 59.0.5 100.00% 59 55

5000 73 43 ' I 1 1 1 1 I 39 6.80 7.00 7.20 _7.40 m/z-> i ■ ■ " • r ’' 51 —H— TTT 4+ i — H __________ 100 I‘‘‘I‘‘‘‘ANA*N**‘‘m 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 55.00 77.42% Abundance #63531:3-Hexanol 59 55

5000 73 .... (N../, "Pun ___ 6.80__ 7.00__ 7.20 7.40 43 m/z 73.00 45.84% 39 i■■ ■ ■ iv" 'I’’ ’ I T ।■■ ■ ■ । +4 11" 11" 69 . " I" TT I ""l'" 'I i" " i11" i11111 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85.90 95 100 105 Abundance . - ! 55 - 43 73 ___ 6.80 7.00 7.20 7.40______ 5000 27 m/z 43.05 34.22% 31 38 i ■ "' i r ■■ ■ i1 i " ■ ■ i ■ " ' i " ■' i ■''' i " " i ■'1' i'''' i " ■ ■ i ■'11 r ■' ■ i' " ■ i " ■ ■ r ■ " i . . / y T| I . I I | m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62540: 1 -Propanamine, 2-methyl- 30 6.80 7.00 7.20 7.40___ m/z 41.00 22.65% 5000 ... 43 73 55 "I"" p"' I»■ i ■ 11 Th i ' i ■ ■ ■ i • ■ ■ i " ■ i" ■ ■ ' ' r ■ ■ i •" T’rm 1 ■ i u ■

m/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.80 7.00 7.20 7.40

1043.D GCMS0208.M Wed Feb 20 14:29:15 2002 Page 3

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