GCMS quantitation results for sample AE04031, March 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAR2202\4031.D Vial: 37 Acq On : 24 Mar 2002 5:36 am Operator: Sample : gc/ms scan 2/25 fb Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Pentane, 3-methoxy- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.15 0.42 ug/1 51013 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 3-methoxy- 102 C6H14O 036839-67-5 9 2 N-Ethyl formamide 73 C3H7NO 000627-45-2 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 4 3,,4-Dimethyl-5-hexen-3-ol 128 C8H160 000000-00-0 4 Abundance Scan 339 (8.154 min): 4031.D (-) m/ z 73.00 100.00% 73 5000 43

87 103 7.80 8.00__ 8.20 8.40_______ ' 1 I 1 1 1 1 1 1 ' i 1 1 1 । I,1 I ' I ‘ 1 i , ' 55, 1 i ।I 1,1 i ■ ‘ 1 ■ i 1 • ■ ■ i ■ * • ’ ■ i ■ ■ 1 > l > ■ ■ ■ • l । m/z 43.0.5 29.28% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance Pentane, 3-methoxy- 73

5000 1 1 I ' ‘ - TM - 45 7.80 8.00 _ 8.20 8.40_______ m/ z 41.05 11.69% .......... 2733 39 TT | I I 1 > | I I I ! | I I 55 ' ' I ' ' ' 1 i 1 1 ■ ■ I ■ 1 1 ■ i 1 ‘ 1 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 IT 1 m/z->10 20 30 40 50 60 70 80 90 100 110 Abundance 30 73 A— 7.80 8.00 8.20 8.40 ___ 5000 m/ z 45.05 10.30% 44 58

15

:m/z->____ _10... 20 .. 30 40 ___50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyi- 30 7.80 8.00 8.20 8.40 m/z 71.0,0 7.57% 5000

15 I 41 , 55 70 87 — 1 1 i 1 t । > । ■ i■> । । । । । । । । । । । । । । । । । । ■ j ■ ■ - ■ । ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

4031.D GCMS0308.M Tue Mar 26 10:44:40 2002 Page 1

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