NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAY0202\LB.D Vial : 3
Acq On 2 May 2002 4:42 pm Operator:
Sample GC/MS SCAN 4/19 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library . : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
8.09 0.71 ug/1 58666 1,4-Dichlorobenzene-d4 12.19
Hit# of 5 . Tentative ID MW MolForm CAS# Qual
1 3-Pentanbl, 3-methyl- 102 C6H140 000077-74-7 33
2 l-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9
3 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9
4 Butane/ 2-methoxy-2-methyl-_____ 102 C6H140 000994-05-8 9
Abundance / Scan 333 (8,089 min): LB.D (-) m/ z 73.10 100.00%
/ 7)3
5000
43
iiir । । i m । ii m । i i i i । i i i i
7.80 8.00 8.20 8.40
.............................. 36 I I I 55 ......... । , 87 103 m/z 43.05 27.91%
1 I | I I I I | I I I ! | I I । i | I r r । । r i i i । i । i i । । I I I k I I I I I 1 I I I 1 T I I
m/z-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #63572: 3-Pentanol, 3-methyl-
73
1 1 ' I 1 1 1 ‘ I 1 ~ 1 I 1 il’1l I I > I I
5000
55 7.80 8.00 8.20 8.40
45 m/z 41.05 12.52%
87
27 |
m/z->
T I r I I I
10
I |
20
I 1 ! ! | >
30
I I I |
40
I ! ! I |
50
I r +
60 70
1 I I [ PH | I | | | | । । | | | r
80 90 100 110
Abundance #763:1 -Butanamine, 3-methyl-
33
"1 1 1 ■ 1 TTITr . > | i TV- | I I i 'l
7.80 8.00 8.20 8.40
5000 m/ z 45.05 12.10%
15, . , T I I
41 , 55 70 87
| I I I I | I ! ’ ! — I I I I | I I I I [ I I ! ’! [ I । I I | 1 I I I [ r
m/z-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #1793: Pentane, 3-methoxy- /
73 7.80 8.00 8.20 8.40
m/ z 71.10 6.36%
5000-
45
... 77 33 39
711*1 "111111‘‘L1 1 i ■
55
11 'i TH ! ■ 1 । ■ ■ ■ ■ । । ■ ■ ■ ■ । ■
m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40
LB.D GCMS0501.M Fri May 03 08:42:39 2002 Page 1
NYC-WTC_000043170
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