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GCMS blank analysis results, sample AE09450, May 3, 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP Box 25 showing GCMS blank analysis of sample AE09450 with semi-volatile organic compounds below detection limits from May 3, 2002.

NYC-WTC_000043164–000043173

Folder label: “GCMS X 4/19/02 A 5/2/02

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Scanned page image, NYC-WTC_000043170
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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0202\LB.D Vial : 3 Acq On 2 May 2002 4:42 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library . : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.09 0.71 ug/1 58666 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 . Tentative ID MW MolForm CAS# Qual

1 3-Pentanbl, 3-methyl- 102 C6H140 000077-74-7 33 2 l-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9 4 Butane/ 2-methoxy-2-methyl-_____ 102 C6H140 000994-05-8 9 Abundance / Scan 333 (8,089 min): LB.D (-) m/ z 73.10 100.00% / 7)3

5000 43 iiir । । i m । ii m । i i i i । i i i i

7.80 8.00 8.20 8.40 .............................. 36 I I I 55 ......... । , 87 103 m/z 43.05 27.91% 1 I | I I I I | I I I ! | I I । i | I r r । । r i i i । i । i i । । I I I k I I I I I 1 I I I 1 T I I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- 73

1 1 ' I 1 1 1 ‘ I 1 ~ 1 I 1 il’1l I I > I I 5000 55 7.80 8.00 8.20 8.40 45 m/z 41.05 12.52% 87 27 | m/z-> T I r I I I

10 I |

20 I 1 ! ! | >

30 I I I |

40 I ! ! I |

50 I r + 60 70 1 I I [ PH | I | | | | । । | | | r 80 90 100 110 Abundance #763:1 -Butanamine, 3-methyl- 33 "1 1 1 ■ 1 TTITr . > | i TV- | I I i 'l 7.80 8.00 8.20 8.40 5000 m/ z 45.05 12.10%

15, . , T I I 41 , 55 70 87 | I I I I | I ! ’ ! — I I I I | I I I I [ I I ! ’! [ I । I I | 1 I I I [ r

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- / 73 7.80 8.00 8.20 8.40 m/ z 71.10 6.36% 5000- 45

... 77 33 39 711*1 "111111‘‘L1 1 i ■ 55 11 'i TH ! ■ 1 । ■ ■ ■ ■ । । ■ ■ ■ ■ । ■

m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

LB.D GCMS0501.M Fri May 03 08:42:39 2002 Page 1

NYC-WTC_000043170

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NYC-WTC_000043170Source: NYC Law Department, mirrored locally

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