GCMS Sample AE03435 Report, March 12 2002

NYC 9/11 Public Portal Document L 1 DL a y

Data File : C:\HPCHEM\1\DATA\FEB21O2\3435.D Vial: 55 Acq On : 23 Feb 2002 10:17 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 3.83 ug/1 266519 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual _________________ A

1 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 28 2 Silane J tetramethyl- 88 C4H12Si 000075-76-3 28 3 1,3-Didxolane, 2-methyl- 88 C4H802 000497-26-7 9 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 Abundance I Scan 344 (8.204 min): 3435.D (-) ........................ ;..m/z 73.00 10 0.00% - 73 |

5000 43

103 { 7.80 8.00 8.20 8.40 8.60 i ■ 1 । I 1 1 1 1 I 38 1 I . 51 — TT10GmCUI ,57, . . STP0IT 67,1 , 87 m/z 43.05 28.77%' m/Z- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 12/03/07/7 7.80 8.00 8.20 8.40 8.60 45 55 m/z 41.05 10.96% 27 39 87 TIT *I111*I’*’(* m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 73 ......... 1 7 7.80 8.00 8.20 8.40 8.60 5000- m/ z 45.05 10.78%

45 15 31 55 88 1 1 I ' ' ' 1 i ' ' ■ 1 j 1 1 * 1 , 1 ■ 1 । । । । । । । । ■ । i J ' । । i । । । । ' , ' ' । । । । । । ' । । m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl- i ' ' ' ' i ‘ ' 1 1 i ■ ' 73 7.80 8.00 8.20 8.40 8.60 m/z 71.0.0 7.06% 5000 43 I 58 27 87 1 ! I ' ' ' ‘ I ' ' ' ' I ' 1 ' 1 I +TT — —— ....... i...................... | ' i ' 1 ■ 1 1 1 1 ' 1 i 1 1 1 1 i ' ............. /, Sr,........ m/Z--) 10 20 30 40 50 60 70 80 90 100 110‘ 7.80 8.00 8.20 8.40 8.60

3435.D GCMS0208.M Fri Mar 08 09:48:46 2002 Page 1

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