GCMS analysis results, sample AE09450, May 8, 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0202\9450.D Vial: 9 Acq On 2 May 2002 10:38 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.08 0.74 ug/1 58966 1,4-Dichlorobenzene-d4 12.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane/ tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane, 3-methoxy-_____________ 102 C6H140 036839-67-5 9 Abundance 7 Scan 332 (8.084 min): 9450.D (-) m/z 73.10 100.00% 73

5000 43

..................................... 36 , J , | | 49 55 ........... | 87 7.80 8.00 8.20 8.40 103 1 ' i 1 ■ ' ■ i 1 1 1 1 i ■ ■ 1 1 I ‘ 1 1 ■ i 1 1 ' ' i ' ' 1 ' i ' 1 ' ' I ' ' ' I 1 1 1 i ' 1 ' 1 i ‘ m/z 43.05 29.33% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- 73

5000- —I < i r | I I I I [ ! i I I [ i i i i1 | i I I I

7.80 8.00 8.20 8.40 45 55 m/Z 41.10 11.63% 27 87 .................. I , 39, | 1 i 1 ' 1 1 i 1 1 1' ■ i ' 1 1 '' i 1 1 ' ' i 1 1'1 ■ i 1 ' ' ■ i 1 ■ ' ' i 1

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 33 73 mmmpuipt 7.80 8.00 8.20 8.40 5000 m/z 45.05 11.19% 44 58

15 । I 1 ' ' l 'I , । , An.....S V 1 ' i ■ ‘ ■ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73 7.80 8.00 8.20 8.40 m/ Z 71.10 7.35% 5000-

45 15 ,I !J । । | ।53_ 5911 । > । । । r | 88 । | 11 *,11

m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

9450.D GCMS0501.M Fri May 03 08:41:34 2002 Page 1

NYC-WTC_000043194