GCMS analysis results for sample AD30011, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30012.D Vial: 9 Acq On : 18 Dec 2001 11:54 pm Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.10 ug/1 839282 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol,/3-methyl - 102 C6H140 000077-74-7 36 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentape, 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance / Scan 278 (7.598 min): 30012.0 (J m/ z 73.00 100.00% S 73

5000- 43

87 103 7.20 7.40 7.60 7.80 8.00 38 |, | 50 55 67, । i ■ ' ' ■ i ' • ' ' i 1 1 r' 1 1 1 i ri 1 1 1 1 1 1 1 r I ■ ■ i ■ ■ i1» i . ■ ■ ■ i ■■■ • • i ■ m/ z 43.00 29.94% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000- 7.20 7.40 7.60 7.80 8.00 55 m/Z 41.00 11.12% 45 87 27 i ■ ' ' ■ I ■ ' ' ■ i I , 39, r. 'i' 1 ' • । ■t—i—I—i-1 -i i*| | — m/z--> 10 20 30 40 50 60 70 8090 100 110 Abundance #292: N-Ethylformamide 30 73 i 7.20 7,40 7.60 7.80 8.00 5000- m/ Z 45.05 10.69% 44 58 15 : 1, । ■ ' i ' ' ■ • i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- —— - । /1 । 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.73% 5000-

.. 15 31 45| 55 —————— > TITI . , . । ! II T’H • 1 1 ' T ............. 88............................. m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30012.D GCMS1126.M Tue Jan 15 15:32:27 2002 Page 1

NYC-WTC_000037321