GCMS analysis results, sample AE09450, May 8, 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0202\9450.D Vial: 9 Acq On 2 May 2002 10:38 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.17 9.54 ug/1 758554 1,4-Dichlorobenzene-d4 12.20 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CHCH2C (0) OCH3 100 C5H802 003724-55-8 9 3 5-Hexen-2-one 98 C6H10O 000109-49-9 7 4 Acetone_____ 58 C3H60 000067-64-1 7 Abundance/ Scan 341 (8.166 min): 9450.D (-) m/z 43.05 100.00% 43

5000 59

1‘I‘**ITTIII IUCI i । । । । । 101 7.80 8.00 8.20 8.40 8.60 ....................... 38 II4+ I I I I I I I 53 , I I I I I I I I I I I I I I 69 I ■ l" I I■ I III I 83 I ' I 1 1 I I I I I [ | 1 1 —1 x m/z 59.10 42.32% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydraxy-4-methyl- 43

5000- 59 780 8.00 8.20 8.40 8.60 m/z 58.10 16.29% 27 101 — +49 4 — ———I— 83 m/z-> 10 20 30 40 50 60 70 80 90 1100I, . 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 - 7 80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.21%

58 1 72 100 38,4 ■ ■ । ■ ■ ■ ■ । । ■ ■ ■ ■ । i * m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2one ' 1 । ' 1 1 ' । 1 1 1 1 । 1 ■ i 1 1 1 1 i 1 43 780 8.00 8.20 8.40 8.60 m/z 41.05 6.94%

5000-

27 55 15 50 | 83 98 m/z-> i 1 ' ' r i —38 4 -1x1—————————' “I 1 ' 1 । ' | । 1 ' " । | 1 । 1 । Ir 02/0/0000/0/1 ' 1 । 1 ttanetpr 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9450.D GCMS0501.M Fri May 03 08:41:35 2002 Page 2

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