GCMS analysis results for sample AE01336, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1902\1336.D Vial: 10 Acq On : 19 Feb 2002 7:09 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.34 ug/1 27229 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 5 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 3 2-(2 Bromoethyl )-1,3-dioxolane 180 C5H9BrO2 018742-02-4 4 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 4 Abundance / Scan 345 (8.210 min): 1336 D (-) m/z..... 73 .00 100.00% ! 73

5000 43 7.80 8.00 8.20 8.40 8.60 57 — PT 11 " TTT’TI , 1 ■ I' 87 r ■ ■ ■ 103 i ' i i'''' i m/z 43.05 25.59% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #292. N-Ethylformamide 30 73

5000 — — 44 55 7.80 __ 8.00__ 8.20 8.40 8.60 m/z 41.05 10.99% 15 i ■ ■ ■ ■ i - 11‘1111171017711‘‘11117"11B00‘TTEOTETTTTT‘T‘OOU‘T"1‘7"TT m/2->10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance ■ 30 ■ ■ । ' 1 i 1 1 1 1 i 1 1 7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 8.06%

15 41 55 70 87 IUUITITTTTTT i " " i " '' I " " r '" i TT r " ‘ i " " i' ■'' i " " r " ' i" m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1 7527: 2-(2-Bromoethyl)-1,3 dioxolane r1 ‘I’’’II’’ 73 7.80 8.00 _8.20_ 8.40 8.60 m/z 71.00 7 .31% 5000 45

Trr‘' I 1l .... 57 I " ' ’ I' r'11 107 152 181 i" " i''1 'r-1 ■ ■ । > > > ■ । > 111111 ■ ip ■ ■ ■ । i " " i' " ' i i ■ • ■ 'I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 7.80 8.00 8.20 8.40 8.60

1336.D GCMS0208.M Thu Feb 21 15:28:20 2002 Page 1

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