Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.
NYC-WTC_000043146–000043160Folder label: “GCMS X 4/18/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C: \HPCHEM\1\DATA\MAY0102\9398.D Vial: 16 Acq On 1 May 2002 9:54 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T. 20.79 1.43 ug/1 118562 Acenaphthene-dl0 21.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy- 1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 3-Isopropoxy- 1,1, 1,5,5,5-hexamethyl 354 C12H3404Si4 072182-11-7 25 3 Trisiloxane, 1/1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 23 4 4-Amino-5-imi dazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 7 t Scan 1719 (20.790 min): 9398.D (-) Abundance m/ z 73.10 100.00% 73
5000 147 281 TT TT Tkir I 45 , 327 383.415 20.40 20.60 20.80 21.00 21.20 - I " i | 117 191 221 249 m/z 147.15 33.12% 11 r I । 1 T 11’1/1/1 * 11 । 1 11 । । । i I 1 1 11 1 1 । 1 1 1 । । । । । । । 1 r m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 ..... ... ... p 1 I 1 1 । 1 | 1 1 1 1 | 1 1 1 i । > । 1 1 । 1 r 147 20.40 20.60 20.80 21.00 21.20 m/z 281.10 29.66% fl i— । । । ii i । 1 r-1 t Cl 1 । । 271 21 327 । 1 1 । 1 1 r 1 । i rh r । 1 1 । । । 415 । । । । । । 1’7 r" । [ 519 561 1 “1 t 1 | T
m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49645: 3-lsopropoxy-1,1,1,5,5,5-hexamethyl-3-(trimethylsil 73 281 20.40 20.60 20.80 21.00 21.20 5000 207 m/z 326.95 8.73% 339 A 249 133 177 , I II 1 I,I I II I .......... .. ........................................................... । ' i ■ ■ ■ ■ i ■ ‘ I I I I [ I I 11 I I I I I I I I I I I I "YU I r r
mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet i | 1 1 . । । । । । ph । । । । r 1 1 r-1 ft
73 147 20.40 20.60 20.80 21.00 21.20 m/z 74.10 8.53% 281 5000
369 207 249 m/z--> 11’ 50 100 150 200 250 300 338 .. 350 400 450 500 550 20.40 20.60 20.80 21.00 21.20 r U
9398.D GCMS0501.M Thu May 02 12:04:40 2002 Page 7
NYC-WTC_000043157
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NYC-WTC_000043079
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043726
Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045223
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10432 conducted on May 20, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043058
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09391 with unknown compounds and surrogate data from May 8, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043112
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044723
Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023363
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023148
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023122
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023076
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.989
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NYC-WTC_000043032
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 18 and May 1, 2002.
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NYC-WTC_000043033
Three-page laboratory record detailing GCMS method parameters including drip rates and volumes for samples analyzed in May 2002.
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Four-page document containing GCMS calibration data and response factors for various chemical compounds analyzed on May 1, 2002.
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Eight-page laboratory report showing GCMS reference analysis results for volatile organic compounds analyzed on May 1, 2002.
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