GCMS calibration table for TCLP analysis, May 2002

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Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.

NYC-WTC_000023363–000023371

Folder label: “GCMS X 5/8/02 A 5/9/02”

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Data File C: \HPCHEM\1\DATA\MAY0302\9520.D Vial: 21 Acq On 4 May 2002 9:41 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Acetic acid, 1-methylpropyl es Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 9.95 1.13 ug/1 79996 1,4-Dichlorobenzene-d4 12.19 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetiqacid, 1-methylpropyl ester 116 C6H1202 000105-46-4 17 2 Acetone 58 C3H60 000067-64-1 9 3 2-Butanol, 3-chloro-, acetate, (R@, 150 C6H11C1O2 054192-20-0 9 4 Propane, 1- (1-methylethoxy) - 102 C6H140 000627-08-7 9 Abundance 1 Scan 536 (9.954 min): 9520.D (-) m/z 43.05 100.00%| 43

5000

58 87 । । । । । i । । ।- 1‘1///m111/8. .... ----l । । । । 9.60 9.80 10.00 10.20 . 10.............. 1140 51 Hr TI1 14— 69 1 —TTI । । । । । | 9 m/ z 58.10 19.93%| miz-> 20 30 50 60 70 80 90 100 110 120 Abundance #3301: Acetic acid, 1-methylpropyl ester 43

5000 9.60 9.80 10,00 10,20 56 87 m/ z 87.05 17.79% 29 73 ' ' i ' ' ' ' i ' ' ''' i ■ > 1 1 । । • j ■ ■ I 101 I1' 1 1 1 I 1,1 1 ■ i ' ' ' ■ । 1 1 1 1 । 1 1 ' 1 । 1 । ' 1 । । mlz-> 10 20 30 40 50 60 70 80 90 100 110 12) Abundance #62322: Acetone 43 ' ■ I ' ■ ■ ■ i ■ ■ ■ ■ i 1 ' 1 1 1 1 ' 1 1 1 1 9.60 9.80 10.00 10.20 5000 m/ z 59.10 12.00% 58 27

mfz—> . 10 -l, ' ' 1 ) 1 11 50 20 6030 40 70 I ' ' ' ' i ' ' ' ' i ' ' ' 1 I 1 1 1 1 I 1 1 1 1 1 1 ' ' 1 1 1 80 90 100 110 120 Abundance #9605: 2-Butanol, 3-chloro-, acetate, (R@,R@)- ■ • i ’ 43 9.60 9.8010.00 10.20 m/z 41.15 10.77%|

5000

87 15 27 , 49 55 ' ' i ' 1 ■ ■ I 1 1 ' 1 I 1 1 ' 1 I ' 1' ■ i' ' ■' r1'11' । 63 72 114 1 > ।11 ' ' I ' ' ‘ ' I 1 1 1 ' 1 1 ' 1 1 I ' YAAAEmLAAAA m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 9.60 9.80 10.00 10.20

9520.D GCMS0501.M Tue May 07 09:38:44 2002 Page 2

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