GCMS analysis results for sample AE04242, Mar 2002

NYC 9/11 Public Portal Document

Library Search compound keporL

Data File : C:\MSDCHEM\l\DATA\022802\04242.D Vial: 8 Acq On : 28 Feb 2002 4:43 pm Operator: McLean Sample : GC MS SCAN 2/26 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 2.37 ug/L 742454 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 43 3 Benzeneacetic acid, .alpha., 3,4-. . . 472 C20H4005Si4 037148-65-5 38 4 N-(Trifluoroacetyl)-N,O,O',O’ 1-t... 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 993 (12.083 min): 04242.D (-) m/z 73110 100.00% 73

5000 267 355

11.80 12.00 12.20 12.40 0 —4+ ,125,154,1′23223.1293,323, , , , , . ....... m/z 267.00 45.52% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 --------PPPP 11.80 1 2.00 12.20 12.40 m/z 355.10 38.18%

45 207 323 0 — I r 1ry r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

1 ' i ' ■ ' ' i ' ■ ' ■ i 1 ■ 1 1 i 1 ' 11.80 12.00 12.20 12.40 5000 m/z 356.10 13.02% 267 355 45 103 133 165 193 223 293 323 | 0 ‘ 4 ‘ '1 ' 'I TT i-i TT Tpmmyim । । । । ri । । m/z-> 50 100 150 200 250 300 350 400 450 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73 PTTTTTTT 11.8012.00 12.20 12.40 m/z 268.00 11.09%

5000 355

147 0 47 105 I 193 237 267295 325 384 429457 m/z-> 50 100 150 200 250 300 350 400 450 11.80 12.00 12.20 12.40

04242.D 5080202.M Wed Mar 13 11:11:48 2002 Page 3

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