GCMS analysis results for sample AE04024, Mar 15 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\4024.D Vial: 79 Acq On : 24 Feb 2002 11:45 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 2 Propanenitrile, 3-(methylamino Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.31 0.31 ug/1 21072 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanenitrile , 3 - (methylamino) 84 C4H8N2 000693-05-0 4 2 Acetamide/ 2-cyano- 84 C3H4N2O 000107-91-5 A 3 Nitrous/Oxide 44 N20 010024-97-2 2 4 Carbon/dioxide 44 CO2 000124-38-9 2 Abundance Scan 356 (8.311 min): 4024.D (-) m/z 39.95 100.00% 40 44

5000 A ........... 36 8.00 8.20 8.40_8.60____ + TTT 59 84 T’TTTTTTTTT . rr-rp-i-rrp-ri-rp- ■ । ■ > ■ ■ । ■ ■ ■ ■ । • ■ ■ ■ ।• i' ■ •11 ■ • ■ ■ ।' • •' । ■ • ■ ■ । ■ m/ z 43.95 92.32% m/Z-?___ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #542: Propanenitrile, 3-(methylamino)- 44

5000 8.00 8.20 8.40 8.60 52 m/z 36.00 6.59% 26 30 84 . 11 i 55 ■ 67 i ■ ■ • • i > • • ■ i > • • ■ i • ■ ■ • 11 ■ • ■ i ■ ■. > i ■ ■ ■ ■ i ■ TT ' " i1 H 11 ■ " ' i " " i "1' i ■ " • i " ■ ■ i ■ ■'11 " " i ■ • miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #532; Acetamide. 2-cyano- 44 41 : 8.00 3.20 8.40 8.60 5000 m/z 83.85 5.98%

16 27 30 38, 68 i ' ■84 WMW"WyWW"ur" T*TITmuu,"mTTT 1 I ' " IT rm-fr-n T 'm/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62271: Nitrous Oxide 44 8.00 8.20 8.40 8.60 m/z 39.00 2.79% 5000- 30 14

i'''' i ■ TTTTT ■ ’ r " ' i " ■ l ’ " ' I b ' I ‘ ' I " ‘ ' I " " I " " I 1 " । | । n I | I I | | | | | miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 8.00 3.20 8.40 8.60

4024 .D GCMS0208.M Wed Mar 13 11:39:05 2002 Page 2

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