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GCMS analysis results, sample AD26202, Dec 2001

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of environmental sample AD26202 conducted Dec 5, 2001, identifying unknown compounds.

NYC-WTC_000031088–000031103

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\26202.D Vial: 71 Acq On : 4 Dec 2001 1:21 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Propanone, 1-methoxy- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

7.01 0.55 ug/1 137194 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1 -methoxy - 88 C4H802 005878-19-3 47 2 Butane, 1-mechoxy- 88 C5H120 000628-28-4 9 3 Acetyl hydroxyamino 75 C2H5NO2 000000-00-0 9 4 Isopropyl Alcohol 60 C3H80 000067-63-0 9 Abundance C——Scan 214 (7.011 min): 26202. D (-) m/z 44.95 100.00% 45

5000 61 73 ■ ■ i ' ' ■ ■ i ■ • • ■ i ■ ■ TITt 6.60 6.80 7.00 7.20 7.40 , 88 207 mmmm +7r — ,....j... i,... >i. <।....।. j i... ।..., ।...., TTT m/z 42.95 83.45% miz-> 10 2030405060 70 8090 100110120130140150160170180190200210 Abundance #62920: 2-Propanone, 1-methoxy­ 5

5000 29 58 6.60 6.80 7.00 7.20 7.40 15 m/z 60.95 35.14% .. 88 Tur Tggm miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62933: Butane, 1-methoxy- 45 1 — A , r 4 : iti । r r — i"

6.60 6,80 7.00 7.20 7.40 5000 m/z 73.00 34.28%

15 27 56 m r l*.. 1 + + “———881 I’’IE“ITCIIEIETTOCTCOOIETIEII mlz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #342: Acetyl hydroxyamino *3— • ' i1 ■71 i 1 ■ i ■ • ■ ' i 43 6.60 6.80 7.00 7.20 7.40 m/z 43.95 20.84% 5000

75 ......... 1.. . ............. ............................. m/z-> 10 20 30 40 50 60 70 80 90 100110120 130140 150160 170180 190200210 6.60 6.80 7.66 7.20 7.40

26202.D NP112601.M Tue Dec 04 16:05:34 2001 Page 1

NYC-WTC_000031096

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NYC-WTC_000031096Source: NYC Law Department, mirrored locally

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