GCMS sample AE05151 analysis, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\HPCHEM\l\DATA\MAR3002\5064.D Vial: 36 Acq On : 31 Mar 2002 3:40 am Operator: Sample : gc/ms scan 3/8 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 0.57 ug/1 80913 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol,/3-methyl- 102 C6H14O 000077-74-7 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxoyane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 ®3iL^^'_4TU^?thoxy-2-methyl- _ 102 C6H14O 000994-05-8 9 Abundance / Scan 336 (8.133rnin):’'5664jDp) 7(3 m/z '73'7 00. ... iboTo^

5000 43

87 103 7.80 JLOQ_ 8^0 8.40_____ I I m/ z 43.05 29.16% __ 10 20 30 40 ____ 50 60 70 80 90 100 110 120 Abundance 7)3

5000 l_ _ 7.80 J.OO _8^ 8.40______ 55 m/z 41.05 12.31% 45 ; ! ^-> 10 20 27 I , 30 39, : ' I ' ‘ I ' I ' ' ' ' I ' ' ‘ ' I ‘ ' I ‘ 87 .I 40 50 60 70 80 90 100 110 120 Abundance N-Ethyifomaniide 30 73 —,-r-|A- I 7.80 8.00 8.20 8.40 5000 m/z 45.05 11.58% 44 58 15 I , I __ 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxoiane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet . . . ....... / , p 7)3 __ 7.80 8.00__ 8.20 840______ m/z 71.0,0'” 7.54% 5000 45 36 III 55 109 115 ......................... \A m/2-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

5064.D GCMS0308.M Tue Apr 02 15:37:26 2002 Page 1

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