GCMS calibration table for TCLP method, March 2002

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Instrument output displaying calibration data and surrogate recovery results for sample AE03283.

NYC-WTC_000011460–000011467

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\1\DATA\MAR0102\3283.D Vial: 43 Acq On 3 Mar 2002 5:38 am Operator: Sample gc/ms scan 2/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.30 ug/1 88902 Phenanthrene-dl0 25.73

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene- 2 5-Oxazolecarboxamide, 2-phenyl- 2.777 188 C14D10 188 C10H8N2O2 001719-06-8 039819-42-6 91 47 3 Naphthalene?, 2,6-dimethoxy- 188 C12H1202 005486-55-5 42 4 2-Quinoli carboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 Abundance Scan 2267 (25.854 min): 3283.D (-) m/z 188.10 100.00% 188

5000 / **1+1*‘1****!*1*’ 80 94 25.60 25.80 26.00 26.20 42 54 64 132 146i 160 , mrtn | if r. । i I I > । i H l'| —l —hPTITTTTTTT mHTT — m/z 189.10 12.93% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 25.60 25.80 26.00 26.20 80 94 m/z 184.10 12.31% 66 160 " “ J ‘ ' i' • ■ ■ i ‘ “ i ■' “ i ‘ “ i1 “ • i' ‘11 1 ‘ i ■ " ‘ i “ " i ■ “ ■ i “ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19812: j-xedlecobugeg 2-phenyi 116 144 188 *mm/g 25.60 25.80 26.00 26.20 5000 m/z 80.00 11.59% 89 63 105 ! mppp • i11' ■ i ‘1 • ■ t ■ “ 11 ■ “ ‘ i “ “ i “ ■ ‘ i “ 1 ■ i “ “ i ■' “ i ■ ‘1 ■ i ■ “ ■ I “ ‘ ■ m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- 188 ..JI,,... 25.60 25.80 26.00 26.20 173 m/z 94.00 10.26% 145 5000 102 76 94 114 130 157 111 ■ ‘ ‘11" 1 ‘ i " “ i1 • । ■ i11 •1141'1 ’ 1 11 TIWTmmpH , । — ----- ‘‘1 ‘ mettrij ‘ * miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

3283.D GCMS0208.M Mon Mar 25 12:19:13 2002 Page 2

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