GCMS calibration table for TCLP method, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\3281.D Vial: 41 Acq On 3 Mar 2002 3:39 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.28 ug/1 79450 Phenanthrene-dl0 25.73

Hit# Of 5 ntative ID MW MolForm CAS# Qual

l Phenanthrene -d10 7 188 C14D10 001517-22-2 90 2 Anthracene-d10- 1 188 C14D10 001719-06-8 87 3 5-Oxazolecarboxamide, 2-phenyl- 188 C10H8N2O2 039819-42-6 38 4 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 36 Abundance 7 ’ Scan2267 (25.854 min):3281.D (-) m/z 188.10 100.00% 188

5000 ... r . . 80 94 40 52 66 132 158 i 25.60 25.80 26.00 26.20 mag mjonnij t ITT m/z 189.10 16.83% m/z~> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

V 5000 ‘I T TT-r 25.60 25.80 26.00 26.20 m/z 94.00 16.36% 80 94 160 - m/z->30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance ost r roupp ’. 1............ . ................ 188 .... A.... ...... 25.60 25.80 26.00 26.20 5000 m/z 184.10 13.30% 66 80 94 160 •' i ■ ■ ■ ■ i ‘ ■ i " " i1" 1111" I''11111111111 I ’ * ’ ’ I ’ * ’ ’ I * ’ • • I m ‘ I ‘'1 * I “ ‘ ‘ I T’T m/z->30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19812:5-Oxazolecarboxamide, 2-phenyl- ............................. ................. 188 25*60 25.80 26.00 26.20 116 144 m/z 80.05 13.21% 5000 89 63 105 mpmpr —m l 1 ‘ i ■'111 ■'1 • i “ •' i ‘' - m&-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ......25.60 25.80 26.00 26.20___

3281.D GCMS0208.M Mon Mar 25 12:17:30 2002 Page 2

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