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GCMS unknowns report, DEP Box 15, June 2002

Machine-extracted title · confidence 90%

GCMS analysis results for sample AE12169 dated June 3, 2002, documenting unknown compounds and surrogate recovery.

NYC-WTC_000013843–000013852

Folder label: “GCMS X 5/23/02 A 5/29/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2902\12169.D Vial: 11 Acq On : 29 May 2002 9:11 pm Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 25.57 0.42 ug/1 48960 Phenanthrene-dl0 25.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 50 2 Anthracene -dlO- 188 C14D10 001719-06-8 42 3 5-Oxazol ecarboxamide, 2-phenyl- 188 C10H8N2O2 039819-42-6 38 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 Abundance Scan 2236 (25,570 min): 12169.D (-) m/z 188.10 100.00%| 188

5000

80 94 1 36 44 54 66 , 160 25.20 25.40 25.60 25.80 26.00 TTTTHTHmpmmtmpt • i' “ ‘ i ‘ "11 “ " r ‘ ’1’7 . 1.. m/z 189.10 15.17% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 25.20 25.40 25.60 25.80 2600 80 m/z 80.00 14.67% 94 160 ■i•" ■।‘ । ।। । - 66 mfa-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d1 0- 1118

25.20 25,40 25.60 25.80 26.00 5000 m/z 184.05 12.68%

. 80 94 66 । Tmmmm ' ‘ 111" I' “ ‘ I " " 11 “ ‘ 11' ‘' 11 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19812:5-Oxazolecarboxamide, 2-pheny- ........................................ ...... 116 144 1118 25.20 25.40 25.60 25.80 26.00 m/z 94.00 12.03% 5000 89 63 105 I......................... n *f “ i “'11 * TTTTTT 1 n11 1 “1 ‘ 1' 11144 ’ 14... **841 Wt miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 2500 25.80 26.00

12169.D GCMS0528.M Thu May 30 08:42:58 2002 Page 2

NYC-WTC_000013851

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NYC-WTC_000013851Source: NYC Law Department, mirrored locally

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