GCMS analysis results, Sample AE08434, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1202\8434.D Vial: 23 Acq On : 16 Apr 2002 5:38 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 6.22 ug/1 822372 1,4-Dichlorobenzene-d4 12.23

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 72 2 2-Propanol, 2-methyl- 74 C4H10O 000075-65-0 17 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 3-Hydroxy-2-pentanone____________ 102 C5H10O2 003142-66-3 9 Abundance Scan 344 (8.205 min): 8434.D (-) m/z 42.95 100.00% 4(3

59 5000

101 7.80 8.00 8.20 8.40 8.60 .......................... 38 1 Bi ' pMl 53 , 67 83 I 1 ' ■ ' 1 1 1 1 ITT । < ! ! । । ' ■ । i 1 ' ' r i 1 m/z 59.05 50.69% mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 100.95 22.25% 27 101 83 I I H 1 ' 49III,, —P—Pm 111 n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62572: 2-Propanol, 2-methyl- 59 7.80 8.00 8.20 8.40 8.60 5000 m/z 58.05 16.68% 31 41

............. 26 I , TT11,, —ll, 1 ■ i ' ' 1 1 1 1 1 1 ‘ i ■ 1 > | ■ ■ • > । ■ ■ ■ ■ I । । । I ■ । । > I > n/z-> 10 20 30 40 50 I60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- I 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.83%

5000

101 15 71 27 1 ■ । । i ■ ■ i > । । , , , f I 56 .1 m/z--> 10 20 30 40 50 60 70 80 90 100 110 7.80" 8.00 8.20 8.40 8.60

8434.D GCMS0412.M Wed Apr 17 09:47:59 2002 Page 2

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