GCMS analysis results for sample AE06997, April 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\APR0 4 05\6997.D Vial: 26 Acq On 6 Apr 2002 10:31 pm Operator: Sample gc/ms scan 3/26 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.22 1.06 ug/1 64721 1,4-Dichlorobenzene-d4 12.24 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 40 2 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 5-Hexen-2fone 98 C6H10O 000109-49-9 9 Abundance l Scan 346 (8.221 min): 6997.D (-) m/z 43.05 100.00% 43

59 5000

101 i 1 ■ ■ 1 । 1 1 ' ' । ' 83 7.80 8 00 3.20 8.40 8.60_ 1 1 I ‘ 1 f 1 I I ................ 38 I I I I I ' 1 ' t I 1 ++49— P—T TT +1 m/ z 59.05 51.26% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 3.00 .20 8.40 3.60 21.44% 27 101

m/z-> 1 1 i ' • 10 ' ■ i 20 - 30 40 +4950—+ —60P70 — 80 83 90 - 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 i < i ’ > 7.80 3.00 8.20 8.40 8.60 5000 m/z 58.05 16.41% 45 15 66 73 84 102 1 1 i * । 1 1 1 1 । 1 1 1 1 । ‘ •dd/d/———DT//—1//d///B//.[ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63448: Morpholine, 4-methyl- 43 7.80 8.00 8.20 8.40 8.60 m/ z 41.05 7.38%

5000

71 101 i ' ' ' ' i 1 ■ ' ' i 1 ' ■ 1 i , । ■ i ' ■ 56 i । । | 82 87 93 J ' I ' 1 1 1 i 1 1 1 ' i 1 1 1 1 ■ r1 1 1 ' i ......... TECEDCE1**AMM .....— A ——11* I11T m/z-> 10 20 30 40 50 60 70 80 90 100 110 7 80 8.00 8.20 8.40 8.60

6997.D GCMS0408.M Mon Apr 15 14:44:53 2002 Page 1

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