GCMS analysis results for sample AE01965, April 2002

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Data File C:\HPCHEM\1\DATA\APRO 302\7311.D Vial: 7 Acq On 3 Apr 2002 6:35 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.22 1.52 ug/1 177622 1,4-Dichlorobenzene-d4 12.25 Hit# Of 5 (Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 2 2-Propanol/, 2-methyl- 74 C4H10O 000075-65-0 17 3 CH2=CHCH (O)OCH3 100 C5H802 003724-55-8 10 4 Acetone / 58 C3H60 000067-64-1 9 Abundance Scan 346 (8.224 min): 7311 .D (-) m/z 42.95 100.00% 43

59 5000

101 7.80 8.00 8.20 8.40 8.60 ......... , . 38 |, ! । 51 . — i i i i | i i 1 । | 83 — i > । 1 i i ) — r 1 1 i ' m/z 59.05 51.47% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 101.05 21.03% 15 31 101 I II I II lI [I 83 - I I I I I I I I I I I I I T-r-r-r-rt — —————— m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62572: 2-Propanol, 2-methyl- 59 . /Try, । 7.80 8.00 8.20 8.40 8.60 5000 m/z 58.05 16.46% 31 41

_26 Jr. i । i |l । | >'i /“i | i r i i | i i i i _। i i i I | I I I | | I

Tl/Z-> 10 20 30 40 50 ।60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 [‘‘‘‘I‘+11111|IYI‘ 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 8.31% 5000

58 38 1 I 72 100 i 1 1 ■ ' i 1 ■ 1 ■ i ■ 1 1 1 i 1 */* PTPTT । ■ ■ ■ 1 । 1 ■ —— MAP... m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

7311.D GCMS0403.M Tue Apr 09 13:07:38 2002 Page 1

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