GCMS analysis results for sample AD27624, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27624.D Vial: 13 Acq On 20 Dec 2001 6:52 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 3-Pentanol, 3-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

7.78 0.78 ng/uL 240835 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 3 -Pentanol, 3-methyl- 102 C6H140 000077-74-7 42 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Pentane'.. 3-methoxy- 102 C6H140 036839-67-5 9 4 1,3-Di xolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance ‘ Scan 320 (7.779 min): 27624.D (-) m/z 73.05 100.00% 73

5000 43 --------

55 7.40 7.60 7.80 8.00 8.20 — । । 87 103 i ■ ■ ■ ■ i 1 ■ ' ■ i i ■ ' ■ ■ i "i m/z 43.10 30.02% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000- —4 7.40 7.60 7.80 - 8.00 8.20 55 m/z 45.10 10.91% 45 87 27 3.9, | ,1 , 1 1 1 '' ' I —TT 1 m/z->10 20 30 40 50 60 70 .80 90 100 110 Abundance #292: N-Ethylformamide 30 73 7.40 ---A---------- 7.60 7.80 3.00 8.20 5000 m/ Z 41.10 10.68% 44 58 «...... I

i ‘ 15....... , > i ■ ■ • ■ i • • ■ ■ i > i » • | । miz-> 10 20 30 40 50 60 70 80 90 100 11 Abundance #1793: Pentane, 3-methoxy- 73 7.40 7.60 7.80 .00 3.20 m/z 71.05 6.88% 5000- 45

m/z-> ...... ■ ■ i 10 ' ■ ■ 1 i ■ 20 2733 39_ — ' ■ ' i ' 30 55 r+' ' ■ i 1 ' 40 ’ 50 60 70 । ' 1 i 1 1 ' '"1 1 ’ ■ ' i 1 ■ ' 1 i r 80 90 100 110 4..... AM 7.40 7.60 ■ 7.80 8.00 8.20

27624.D NP112701.M Thu Dec 20 11:39:52 2001 Page 5

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