GCMS analysis results for sample AD27768, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27768.D Vial: 11 Acq On : 20 Dec 2001 5:02 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Pentanol, 3-methyl- • Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

7.78 0.84 ng/uL 281326 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3- methyl- 102 C6H140 000077-74-7 36 2 1, 3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 23 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Pentane, 3-methoxy-__________________ 102 C6H140 036839-67-5 9 ’Abundance Scan 321 (7.782 min): 27768.D (-) m/ z 73.0.5 100.00% 73

5000 43 • i ■ ■ ■ ■ । 1 ----- 57 7.40 7.60 7.80 8.00 8.20 — Trm । । 1......... 87............ 103.................... nr1 m/ z 43.10 32.88% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63573: 3-Pentanol, 3-methyl- 73 I , I I I > — — I — > — 5000 7.40 7.60 7.80 8.00 8.20 55 m/ z 45.10 11.42% 45 87 27 TIr 1 ' ‘T ■ i , TT l’1 39, I . ■ i ■ ■ ■ ■ । ■ — m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1.3-Dioxolane. 2-(3-brorno-5,5.5-trichloro-2,2-dimet 73 — -I 7.40 7.60 7.80 0( 8.20 5000- m/ z 41.10 10.41% 45 36 55 67 109 115 m/z->___ 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 7.40 7.60 7.80 8.00 8.20 73 m/z 71.05 6.62% 5000- 44 58

m/z—> —1-..... 1— 10 20 30 40 50 60 70 80 90 100 110 120 AA 7.40 7.60 7.80 8.00 8.20

27768.D NP112701.M Thu Dec 20 11:46:43 2001 Page 5

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