Laboratory report documenting GCMS analysis of sample AD27986 conducted on January 2, 2002, noting unknown compounds and surrogate recovery.
NYC-WTC_000034472–000034483Folder label: “GCMS X 11/21/01 A 12/21/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC1901\27986.D Vial: 27 Acq On : 21 Dec 2001 7:40 am Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
7.76 0.50 ng/uL 162759 1,4-Dichlorobenzene-d4 11.85
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Pentanol, 3-me, yl- 102 C6H140 000077-74-7 36 2 1,3-Dioxolane, /2 -(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 23 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Pentane,_ 3-methoxy-_________ 102 C6H140 036839-67-5 9 Abundance Scan 318 (7.761 min): 27986.D (-) m/z 73.05 100.00% 73
5000 43 7.40 7.60 7.80 8.00 8.20
miz-> ...... 10 .......... 20 30 -55 40 50 60 II 4 70 80 ; f 87 90 103 100 110 120 m/z 43.10, 31.87% 'Abundance #63573: 3-Pentanol, 3-methyl- 73
5000 ' ' P ■ ■ ' i ' T 1 ■ p 11111 7.40 7.60 7.80 8.00 8.20 55 m/z 10.86% 27 45 87 45.10 39 i 11।* ' p 1 ' ' P TIT Tt 'i' TH ।.... । . I . . । . TT ] । । . m/z—> 10 20 30 40 50 60 70 80 100 110 90 120 Abundance #49423; 1.3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 ■ > । ■ ■ ■ ■ । ■ 7.40 7.60_ 7.80 8.00 8.20 5000 m/z 41.10. 10.19% 45 36 55 67 109115 ■ 1 i ■ ■ ■ ■ i ■ 1 1 ■ i 1 ' ■ ■ i ■ 1 ■ miz-> 10 20 30 40 50 60’ 70 80 190 1100— 110 120 Abundance #292: N-Ethylformamide -................. 30 7.40 7.60 7.80 8.00 8.20 73 m/z 71.05 6.44% 5000 44 58
miz-> —16 10 .... 20 —30 1T ।1 40 50 60 70 80 90 100 110 120 - 7.40 7.60 7.80 8.00 8.20
27986.D NP112701.M Fri Dec 28 09:31:48 2001 Page 1
NYC-WTC_000034480
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NYC-WTC_000034484
Laboratory report documenting GCMS analysis of sample AD28046 conducted on January 2, 2002, noting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034505
Laboratory report documenting GCMS analysis of sample AD28047 conducted on January 2, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034516
Laboratory report documenting GCMS analysis of sample AD28044 conducted on January 2, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034436
Laboratory report documenting GCMS analysis of sample AD27775 conducted on January 2, 2002, noting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035528
GCMS analysis results for sample AD28322 dated January 3, 2002, showing surrogate compound results.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034537
Laboratory report documenting GCMS analysis of sample AD28048 conducted on January 2, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034548
Laboratory report documenting GCMS analysis of sample AD28049 conducted on January 2, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034631
Laboratory report documenting GCMS analysis of sample AD28167 conducted on January 2, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035550
GCMS analysis results for sample AD28324 dated January 3, 2002, showing surrogate compound results.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034642
Laboratory report documenting GCMS analysis of sample AD28105 conducted on January 2, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035411
Laboratory report detailing GCMS results for sample AD28309 analyzed on January 3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032941
Laboratory report documenting GCMS analysis of environmental sample AD27391 conducted on December 19, 2001.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034424
Document page with illegible text and partial date fragments, likely a GCMS record based on folder context.
Filed in the same folder
NYC-WTC_000034425
Fragmented DEP laboratory record from December 2001 containing illegible text and partial date stamps.
Filed in the same folder
NYC-WTC_000034428
Laboratory calibration table for EPA Method 625/TCLP analysis dated December 21, 2001, listing standard compounds and response factors.
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NYC-WTC_000034436
Laboratory report documenting GCMS analysis of sample AD27775 conducted on January 2, 2002, noting unknown compounds and surrogate recovery.
Filed in the same folder
NYC-WTC_000034447
Laboratory report documenting GCMS analysis of sample AD27984 conducted on January 2, 2002, noting unknown compounds and surrogate recovery.
Filed in the same folder