GCMS analysis results for sample AD27632, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27632.D Vial: 20 Acq On : 20 Dec 2001 3:14 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 3-Pentanol, 3-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.77 1.00 ng/uL 268893 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# • Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 1,3 .-Dio: lane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 'Abundance 7 Scan 319 (7.769 min): 27632.D (-) m/ z 73.05 100.00% 73

5000- 43 ---------------- 103 87 7.40 7.60 7.80 8.00 8.20 TTT -H-+ + TTTT TTTTT m/z 43.10 29.55% m/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 55 7.40 7.60 7:80 8.00 8.20 45 87 m/z 45.10 12.15% 27 TTT —1 I •' •' I — T T......... I "'' I I' “' I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1793: Pentane, 3-methoxy- 7.3 i

7.40 7.60 . A7.80 ........ 8.00 8.20 5000 m/ z 41.10 10.74% 45

2733 39 55 | TIIWWWT)WWT)WWTWWTU]NNTTTTTTTPITIWWPTIWWWIIWIDI)TT ’1 r1111'11111"11' •111" m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63573: 3-Pentanol, 3-methyl- —AMPMPFIIATAA 73 7.40 7.60 7.80 8.00 8.20 m/z 71.05 6.72% 5000 55 27 45 87 —

m/z--> 1 TmD 39, 1 > i1' Wp HHmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 7.40 7.60 7.80 3.00 8.20

27632.D NP112701.M Fri Dec 21 09:20:32 2001 Page 5

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