GCMS analysis results for sample AD27764, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC1901\27764.D Vial: 7 Acq On 19 Dec 2001 12:38 pm Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) ' Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hydrogen azide Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

5.00 0.88 ng/uL 222646 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 3 2 Ethylamine 45 C2H7N 000075-04-7 2 3 Acetic acid, anhydride 102 C4H603 000108-24-7 1 4 Propanoic acid, 2-oxo- 88 C3H403 000127-17-3 1 Abundance Scan 17 (4.995 min): 27764.D (-) m/z 43.1 100.00% 43

5000 T’TEIIETITTEEETT 4.90 5.00 5.10 5.20 5.30 5.40 i । rp-m-p- | " । । j । l r . | | ] Tr tr । ... d ,.... ।. । ।. . . . । rr. . । ..i. । iT m/z 44.05 6.22% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance

5000 - 15 #33: Hydrogen azide 43 M I ' ' ' ' I 4.90 5.00 5.10 5.20 5.30 5.40 m/z 42.10

I 29 6.18% • i • ■' • i • ■ I " '' I I ‘" I ।।।. r..।,11,।,.।।,i,।,,,,।....।.11.1 TT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #42: Ethylamine 30 4.90 5.00 5.10 5.20 5.30 5.40

N. 5000 m/z 45.00 4.04% 44 15 27 ! 3841 11 TTTTTT TT 11TTTIIT TTT TTTTTT i. ■. • i ■. ■11 ■ ■ > < i ■ • ■ • i' ■'11 ■ • ■ ■. ■ ■". • • ■ ■ i m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63470: Acetic acid, anhydride PPPr I, ,1 '1' , 43 . 4.90 5.00 5.10 5.20 5.30 5.40

5000

15 29 60 87 —+ •।•••■।• i‘ ■ i'" • i'"' i " " i ■ ’" r "' r " ■ i m/z--> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

27764.D NP112701.M Thu Dec 20 11:43:20 2001 Page 1

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