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GCMS analysis results for sample AD27639, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27639 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033221–000033246

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033230
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\27639.D Vial: 3 Acq On : 18 Dec 2001 5:44 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM.\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 Hydrogen azide Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

5.04 1.10 ng/uL 251226 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 4 2 Acetic acid/ anhydride 102 C4H603 000108-24-7 2 3 Acetic acid, anhydride 102 C4H603 000108-24-7 2 4 1,4-Benzenediol, 2,3-dichloro-5,6-d 312 C12H6C12N2O4 000000-00-0 1 Abundance Scan 22 (5.043 min): 27639.D (-) m/z 43.10 100.00% 43

5000

i ■ ■11111 ■11' ■ • ■ । 11'' ‘ I ’''' I' ’ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 r ■ " i1" ‘ i1' ‘ i — tr TTTTTT TTTTTTTTTTTTTTTTTTTTTTTTT TT m/z 42. 0 6.84% m/z~> 5 1G 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33: Hydrogen azide

5000 15

29 43

TT J 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 44.00 3.21%

m/z--> Abundance ‘I 5 10 15 20 l i " " r "11" " r ■ ■ ■ i'1 25 30 i iT I " " r " ' i" " r 35 40 45 50 55 60 65 #1680: Acetic acid, anhydride 43 r " ■ i ■1" i11" i' " 11" 1 ■ r 70 75 80 85 90 95

‘_____ /W MMA 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- m/z 45.05 1.09%

m/z-> Abundance

5000 29 TTTTTPPmmpp 5__ 10 15 20 25 60 87 iTTTp-rrrp-rTTp-1uI1U10110011101711117117 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #63470: Acetic acid, anhydride 43 uL 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 41 1.07%

15 60 m/z~> 5 wk I' •' • I 29 TIT TH + 11111 p-rrrfrrrrp-rnTWPIUTTT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 87 1 • TTTT 1‘ i 1 ' ' ■ T' ' 4.90 5.00 5.10 5.20 5.30 5.40 5.50

27639.D NP112701.M Thu Dec 20 11:36:54 2001 Page 1

NYC-WTC_000033230

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NYC-WTC_000033230Source: NYC Law Department, mirrored locally

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