GCMS analysis results for sample AD27639, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\27639.D Vial: 3 Acq On : 18 Dec 2001 5:44 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Oxepane, 2,2,4-trimethyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.12 2.00 ng/uL 457606 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxepane, 2 ,2,4-trimethyl- 100 C6H120 023120-44-7 39 2 1-Pentanol/ 4-methyl- 102 C6H140 000626-89-1 33 3 1-Hexene / 84 C6H12 000592-41-6 33 4 Pentanal, 3-methyl-_______________ 100 C6H120 015877-57-3 23 Abundance 7 Scan 30 (5.116 min): 27639.D (-) m/ z 41.10 100.00% 41 56

5000

45 71 11' ‘ '11' •' 111 ‘ • l11 ‘‘I ’ 4.90 5.00 5.10 5.20 5.30 5.40 5.50

miz—> 37 I — TIITTTTTTTTTTT 51 TTTUr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 50 1.511111 100 TTTTrr 95 100 105 m/ z 56 10 74.23% Abundance #1525: Oxepane, 2,2,4-trimethyl- 43 59

5000 f 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 59 10 65.47%

m/z-> '' r " ' i ‘ 31 . i Tp TTm-rp-r i ■ ■ • ■ i 5485 100 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63578; 1-Pentanol, 4-methyl- 56 41 T‘ TT T‘ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 69

N 5000 m/z 42 __ 10 64.70%

45 i I 60 84 TT Thr ' i " " I "'111 TTTumuuupuga m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62755: 1-Hexene 41 56 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 m/z ,43.10 62.28% 5000- 84 69

m/z-> TTyrrTTp- TITTTrT 20 25 —5l+ TTTTT r ■" i' " ' i 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 p-rTT [ rm-p-m-p nip TTTI 4.90 5.00 5.10 5.20 5.30 5.40 5.50

27639.D NP112701.M Thu Dec 20 11:36:56 2001 Page 2

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