GCMS analysis results for sample AD27765, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\27765.D Vial: 8 Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Oxepane, 2,2,4-trimethyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

5.10 1.38 ng,/ uL 309447 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 entative ID MW MolForm CAS# Qual -------- ---- 7------------ - 1 Oxepane, 2, 2,4-trimethyl- 100 C6H120 023120-44-7 36 2 l-Hexene/ 84 C6H12 000592-41-6 33 3 1-Hexene 84 C6H12 000592-41-6 33 4 Hexylene Glycol 118 C6H14O2 000107-41-5 10 Abundance / Scan 28 (5.098 min): 27765.D (-) m/z 41,10 100.00% 41 56

5000

71 r ■'' i ■' ■' i1 - " r ■ " i' • ■' i 1111' I j 50 । | 77 82 109 4.90 5.00 5.10 5.20 5.30 5.40 5.50 93 — TTTTTTTTT I ‘1 "I TVTTTTTTP m/z 56.10 77.44% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 115 Abundance #1525: Oxepane, 2,2,4-trimethyl- 43 59

5000 TOIUEpT TTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 59 70.75% 85 m/z-> + 31 ' "' I ‘ " I''" I ' ' 100 ' TT I" ■r 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 >05 110 115 r ■" i" " r " r " i " " i Abundance #62755: 1-Hexene 41 56 27 i ■ ■ ■ ■ । mmn 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- m/z 42.10 59.53% 84

AaL 69 51 r "11 ’1 1‘U"OEEO"TEIII""I‘TT O‘IE‘1U0011UUU10U11TEETTI‘TTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #62753:1-Hexene > 111.1 > I TTT . I.... 1 < TTTTm 41 56 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z. 43.10 52.15% 5000 27 84 69

TTT TTTTS-rrrp-rT i" " r "' r " I""I ■"'r"' i""r"' i""r11 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 4.90 5.00 5.10 5.20 5.30 5.40 5.50

27765.D NP112701.M Thu Dec 20 11:23:30 2001 Page 2

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