GCMS non-target scan comment, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26203.D vial: 26 Acq On : 1 Dec 2001 10:56 am Operator: GALOS Sample : gc/ms unknown 11/3 reext Inst : GC/MS Ins Mise ♦ Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hydrogen azide Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.40 ng/uL 121906 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hydrogen azide 43 HN3 007782-79-8 4 2 Ethylamine 45 C2H7N 000075-04-7 2 3 Acetic acid, anhydride 102 C4H603 000108-24-7 2 4 Acetic acid, anhydride 102 C4H6O3 000108-24-7 1 Abundance Scan 18 (5.010 mir 203.D (-) m/z 43.00 100.00% 43

5000

T p.M p.. IjM M ]. ’211 » i i i j 4.90 5.00 5.10 5.20 5.30 5.40

M. 56 m/z 42.00 5.51% 11 ■ • ■ TIUTTI... ।. 11—00090731 miz-> 5 10 15 20 25 30 3 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33: Hydrogen azide 43

5000 15 -AMA 4.90 5.00 5.10 5.20 5.30 5.40 29 44.00 2.95% 1 1— 1‘ miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #42: Ethylamine 33 ।■■■■।■• “ ।1 “ •।■■ •' । । । 4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z45.00 2.48%

mz-> Abundance

5000 15 27 44 3841 ................................. ’’I’’ - ir111001111111011110 111117 TIITTT —2101011171 TIEUCTI0—TTT0""’’1" 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #1680: Acetic acid, anhydride 43 MA 4.90 5.00 5.10 5.20 5.30 5.40 m/z38.10 i ■ ■1 ■ i

0.89%

29 1 ,।।।।11, ।. 11।11 j i H . ।।j।.t«... j.... j।।. 60 87 T ’II ’1t■ I TT-n-p-rr "I-—21T m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.90 5.00 5.10 5.20 5.30 5.40

26203.D NP112701.M Tue Dec 04 15:05:58 2001 Page 1

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